| 4,5—亚乙二硫基—1,3—二硫杂环戊烯—2—酮衍生物的合成 |
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| 引用本文： | 赵富录 王小刚. 4,5—亚乙二硫基—1,3—二硫杂环戊烯—2—酮衍生物的合成[J]. 西北大学学报(自然科学版), 1998, 28(1): 41-43 |
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| 作者姓名： | 赵富录 王小刚 |
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| 作者单位： | 西北大学化学系 |
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| 摘 要： | 以二（１，３－二硫杂环戊烯－２－硫酮－４，５－二硫）合锌酸四乙基铵盐（Ｉ）为原料，合成四种未见文献报道的４，５－亚乙二硫基－１，３－二硫杂环戊烯－２－硫酮及酮ＩＶａ，ＩＶｂ，Ｖａ，Ｖｂ，其中由路线Ａ和Ｂ分别制得了Ｖａ；对ＩＶｃ和由路线Ａ制备Ｖｂ失败的原因进行了讨论。
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| 关 键 词： | 4.5－亚乙二硫基－1.3－二硫杂环戊烯－2－酮衍生物；4.5－亚乙二硫基－1.3－二硫杂环戊烯－2－硫酮衍生物；双（亚乙二硫基）四硫富瓦烯中间体合成 |
Synthesis of 4,5 ethylenedithio 1,3 dithiole 2 one Derivatives |
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| Zhao Fulu Wang Xiaogang Wang Jianhua. Synthesis of 4,5 ethylenedithio 1,3 dithiole 2 one Derivatives[J]. Journal of Northwest University(Natural Science Edition), 1998, 28(1): 41-43 |
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| Authors: | Zhao Fulu Wang Xiaogang Wang Jianhua |
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| Abstract: | ethylenedithio 1,3 dithiole 2 ones IV a, IV b,V a,V b were prepared from Bis(tetraethylammonium) bis (2 thioxo 1,3 dithiole 4,5 dithiolate)Zincate(I), The compound V a have been prepared through route A and B. Attamput of synthesis of IV c and V b from route A was unsuccessful, The reason for lack of the expected products was discussed. |
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| Keywords: | ethylenedithio 1 3 dithiole 2 one 4 5 ethylenedithio 1.3 dithiole 2 thione BEDT TTF intermediate synthesis |
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