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用Sol-gel法制备掺杂的锶铁氧体的结构研究
引用本文:黄凯,吕建国.用Sol-gel法制备掺杂的锶铁氧体的结构研究[J].安庆师范学院学报(自然科学版),2009,15(3):67-69.
作者姓名:黄凯  吕建国
作者单位:安徽建筑工业学院,数理系,安徽,合肥,230601;安徽大学,物理与材料学院,安徽,合肥,230039
摘    要:采用溶胶-凝胶法(Sol-gel法)制备镧钴掺杂的纳米锶铁氧体(Sr1-xLaxFe12-yCoyO19),使用X射线衍射仪、振动样品磁强计、阻抗自动测量仪(LCR电桥)对掺杂的锶铁氧体进行表征,对其结构、相变进行研究。实验结果表明,温度高于850℃时样品为稳定的M相结构,在掺杂的样品中发现了磁导率减落现象,证实了Co^2+离子进入到六角晶体的晶位中。

关 键 词:锶铁氧体  掺杂  磁导率减落

Structural Analysis for Preparing Substituted Sr Hexaferrite Nanoparticles by Sol-gel Method
HUANG Kai,LV Jian-guo.Structural Analysis for Preparing Substituted Sr Hexaferrite Nanoparticles by Sol-gel Method[J].Journal of Anqing Teachers College(Natural Science Edition),2009,15(3):67-69.
Authors:HUANG Kai  LV Jian-guo
Institution:1.Department of Mathmatics & Physics;Anhui University of Architecture;Hefei 230601;2.School of Physics & Materials Science;Anhui University;Hefei 230039;China
Abstract:Sr1-xLaxFe12-yCoyO19 is prepared to characteristic Sr Hexaferrite Nanoparticles and study their structure and phase-varying by sol-gel method and by means of X-ray diffraction(XRD),vibrating sample magnetometer and LCD bridge with computer aided system.The experimental results show that the samples are steady M-phase when temperature is beyond 850℃,and magnetic disaccommodation can be obviously found in the substituted Sr hexaferrite nanoparticles.So,this behaviour shows that the magnetic Co2+ ionic go into the crystal of hexagonal structure.
Keywords:strontium ferrites  substitution  magnetic disaccommodation  
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