| 基于TGA-FTIR联用技术的PVC热解研究 |
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| 引用本文： | 周琥,陆继东,周浩生. 基于TGA-FTIR联用技术的PVC热解研究[J]. 华中科技大学学报(自然科学版), 2000, 28(9): 82-83 |
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| 作者姓名： | 周琥 陆继东 周浩生 |
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| 作者单位： | 华中理工大学煤燃烧国家重点实验室 |
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| 摘 要： | 用TGA-FTIR联用的方式进行了PVC在空气条件下的热解实验,分别用DDTG曲线与FTIR的红外三维图、Gram-Schmidt(GGs)曲线等描述了PVC两个阶段的热解行为,对比了DDTG曲线与GGs曲线中峰的位置以及峰的起始时间、终止时间、峰宽等参数,结果表明,TGA与FTIR联用时,FTIR的检测无明显的滞后,及返混等情况发生.
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| 关 键 词： | 聚氯乙烯 热解 热重-红外联用分析 |
| 文章编号： | 1000-8616(2000)09-0082-02 |
| 修稿时间： | 1999-12-28 |
Study of the Prolysis of PVC with the Coupling of a TGA and FTIR |
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| Zhou Hu Lu Jidong Zhou HaoshengState Key Lab. of Coal Combustion,HUST ,China.. Study of the Prolysis of PVC with the Coupling of a TGA and FTIR[J]. JOURNAL OF HUAZHONG UNIVERSITY OF SCIENCE AND TECHNOLOGY.NATURE SCIENCE, 2000, 28(9): 82-83 |
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| Authors: | Zhou Hu Lu Jidong Zhou HaoshengState Key Lab. of Coal Combustion HUST China. |
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| Affiliation: | Zhou Hu Lu Jidong Zhou HaoshengState Key Lab. of Coal Combustion,HUST 430074,China. |
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| Abstract: | The prolysis characteristics of the polyvinyl chloride (PVC) in air are investigated by means of coupling of a Fourier transform infrared (FTIR) spectrometer to a thermogravimetric analyzer (TGA). It is observed that PVC is reduced in two stages in air. The analysis of FTIR is contrasted with TGA. It is proved that TGA FTIR is a powerful technique. |
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| Keywords: | Polyvinyl chloride prolysis TGA FTIR |
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