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正交试验考察新疆锁阳中总黄酮的提取工艺
引用本文:康新平,热娜·卡斯木,龚兰新. 正交试验考察新疆锁阳中总黄酮的提取工艺[J]. 新疆师范大学学报(自然科学版), 2008, 27(3): 70-72
作者姓名:康新平  热娜·卡斯木  龚兰新
作者单位:[1]新疆医科大学药学院,新疆乌鲁木齐830054; [2]新疆师范大学生命科学与化学学院,新疆乌鲁木齐830054
基金项目:新疆自治区卫生厅青年科技人才专项基金
摘    要:以芦丁为对照品,用分光光度法比较醇提法、超声法、煎煮法从锁阳干燥肉质茎中提取有效成分黄酮类化合物的提取效率。采用正交试验优化了超声法的提取工艺。结果表明料液比和超声时间对黄酮类化合物的提取效率有显著影响,乙醇浓度对提取效率影响不显著。得到最佳提取工艺为60%乙醇、1:60料液比、超声1.5h。

关 键 词:锁阳  黄酮类化合物  最佳提取工艺  超声

On the Extraction Technology of the Total Flavones of Xinjiangs Cynomorium Songaricum Rupr.
KANG Xin-ping,Rena KASIMU,GONG Lan-xin. On the Extraction Technology of the Total Flavones of Xinjiangs Cynomorium Songaricum Rupr.[J]. Journal of Xinjiang Normal University(Natural Sciences Edition), 2008, 27(3): 70-72
Authors:KANG Xin-ping  Rena KASIMU  GONG Lan-xin
Affiliation:KANG Xinping, Rena KASIMU, GONG Lanxin, (1. College of Pharmacy, Xinjiang Medical University ,Urumqi Xinjiang 830054; 2. School of life Science and Chemistry, Xinjiang Normal University, Urumqi Xinjiang 830054)
Abstract:To ascertain the optimum condition for extracting Cynomorium Songaricum Rupr, the authors of this paper take rutin as a comparison and compare the extraction methods of the total flavones of Cynomorium songaricum Rupr, and study the optimal conditions for extracting flavonoid compounds of Cynomorium songaricum Rupr with the help of L9 (34) orthogonal table. The volume of alcohol and the time of extraction affect the total flavones significantly. The results show that the highest extraction rate of the total flavones could be obtained with 60% ethanol solution at a ratio of solid to liquid 1:60 and ultrasound 1.5 h.
Keywords:Cynomorium Songaricum Rupr.  total flavones  the optimum extraction process  ultrasound
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