| 云南植物药萝芙木中51种农药残留的测定 |
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| 引用本文： | 李家雄,范伢,李桂镇,熊佳梁,王红斌,袁燕.云南植物药萝芙木中51种农药残留的测定[J].云南民族大学学报(自然科学版),2015(3):194-198. |
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| 作者姓名： | 李家雄 范伢 李桂镇 熊佳梁 王红斌 袁燕 |
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| 作者单位： | 云南民族大学民族药资源化学国家民委-教育部重点实验室 |
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| 基金项目： | 云南民族大学绿色化学与功能材料研究省创新团队项目(2011HC008);云南省高校绿色化学新能源与材料科技创新团队项目(2011UY09);2012年国家级大学生创新创业训练计划项目(201210691001);民族药资源化学国家民委-教育部重点实验室开放基金(MZY1122) |
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| 摘 要： | 用超高效液相色谱(UPLC)、双柱毛细管气相色谱(GC)、高效液相色谱-二级质谱(HPLC-MS/MS)分析方法对云南萝芙木进行51种农药残留测定.各测定方法在一定范围内线性关系良好,准确度和精密度均符合农残分析要求,在超高效液相色谱和高效液相色谱串联二级质谱中仅检测出多菌灵,含量分别为0.012 mg·kg-1和0.018 mg·kg-1,未超出国家食品中农药最大残留限量标准,没有检出其它50种农药.
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| 关 键 词： | 农药残留 固相萃取 超高效液相色谱 气相色谱 萝芙木 |
Determination of 51 kinds of pesticide residues in Yunnan rauvolfia |
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| LI Jia-xiong;FAN Ya;LI Gui-zhen;XIONG Jia-liang;WANG Hong-bin;YUAN Yan.Determination of 51 kinds of pesticide residues in Yunnan rauvolfia[J].Journal of Yunnan Nationalities University:Natural Sciences Edition,2015(3):194-198. |
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| Authors: | LI Jia-xiong;FAN Ya;LI Gui-zhen;XIONG Jia-liang;WANG Hong-bin;YUAN Yan |
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| Institution: | LI Jia-xiong;FAN Ya;LI Gui-zhen;XIONG Jia-liang;WANG Hong-bin;YUAN Yan;Key Laboratory of Chemistry in Ethnic Medicinal Resources,State Ethnic Affairs Commission and Ministry of Education of China,Yunnan Minzu University; |
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| Abstract: | This research used an ultra high-performance liquid chromatography( UPLC),and double column capillary gas chromatography( GC),and high-performance liquid chromatography-the secondary mass spectrometry( HPLC-MS / MS) to determine 51 species pesticide residues in Yunnan rauvolfia samples. The results showed that the above-mentioned methods had the features of a good linear relationship,precision,stability and reproducibility. Only carbendazim among the 51 kinds of pesticides in the samples was detected by UPLC and HPLC-MS /MS. Its content was 0. 012 mg·kg-1and 0. 018 mg·kg-1respectively. The content in this sample did not exceed the limits of the maximum residue standards for food in China. Other 50 kinds of pesticides were not detected. |
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| Keywords: | pesticide residues solid phase extraction UPLC GC rauvolfia |
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