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溶胶-凝胶-水热法制备Na0.5Bi0.5TiO3单晶纳米棒的研究
引用本文:夏华婷,胡永明,周迪,王钊,郭鹏,陶毅博,许杨,顾豪爽.溶胶-凝胶-水热法制备Na0.5Bi0.5TiO3单晶纳米棒的研究[J].湖北大学学报(自然科学版),2011,33(2):149-151,196.
作者姓名:夏华婷  胡永明  周迪  王钊  郭鹏  陶毅博  许杨  顾豪爽
作者单位:湖北大学物理学与电子技术学院,铁电压电材料与器件湖北省重点实验室,湖北武汉430062
基金项目:国家自然科学基金,教育部博士点基金
摘    要:采用溶胶-凝胶-水热法在一定条件下合成单晶Na0.5Bi0.5TiO3纳米棒.该方法能够很好地控制产物的组分,避免高温晶化过程中Na或Bi离子的挥发.利用XRD、SEM、TEM和紫外/可见吸收光谱等分别对产物的物相、形貌、微结构以及光吸收等性质进行表征.结果表明获得的产物为三方相钙钛矿结构,NBT纳米棒与NBT粗晶材料...

关 键 词:Na0.5Bi0.5TiO3  纳米棒  溶胶-凝胶-水热法

Study of Na0.5Bi0.5TiO3 single crystal nanorods synthesized by sol-gel-hydrothermal method
XIA Huating,HU Yongming,ZHOU Di,WANG Zhao,GUO Peng,TAO Yibo,XU Yang,GU Haoshuang.Study of Na0.5Bi0.5TiO3 single crystal nanorods synthesized by sol-gel-hydrothermal method[J].Journal of Hubei University(Natural Science Edition),2011,33(2):149-151,196.
Authors:XIA Huating  HU Yongming  ZHOU Di  WANG Zhao  GUO Peng  TAO Yibo  XU Yang  GU Haoshuang
Institution:(Key Laboratory of Ferro-Piezoelectric Materials and Device of Hubei Province,School of Physics and Electronic Technology,Hubei University,Wuhan 430062,China)
Abstract:Single crystal Na0.5Bi0.5TiO3 nanorods were synthesized by a novel method of sol-gel-hydrothermal under certain conditions.The advantages of this method included the controllability of elements composition and non-volatilization for Bi and Na ions.The phase,morphology,microstructure and optical absorption property were characterized by using XRD,SEM,TEM and UV/vis absorption spectrum technologies.The results showed that the as-prepared Na0.5Bi0.5TiO3 nanorods were thombohedral perovskite phase,with the energy band of about 3.38 eV.Blue shifts happened with the UV/vis absorption spectrum as comparing the Na0.5Bi0.5TiO3 nanorods with macrograin materials.
Keywords:Na0  5Bi0  5TiO3  nanorod  sol-gel-hydrothermal method
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