| 以TNT为原料合成均苯三酚三甲醚 |
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| 引用本文： | 胡益民,王修然. 以TNT为原料合成均苯三酚三甲醚[J]. 安徽师范大学学报(自然科学版), 1999, 22(1): 53-55 |
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| 作者姓名： | 胡益民 王修然 |
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| 作者单位： | 安徽师范大学有机化学研究所,安徽,芜湖,241000 |
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| 摘 要： | 均苯三酚三甲醚是新型医药及农药合成的中间体，国内外需求量较大，目前国内尚无生产。据此我们提出以ＴＮＴ为原料经氧化、还原、水解、醚化四个步骤合成标量化合物。本方法具有产率高、操作简便、原料价廉以及污染较少，适宜转化工业生产，有一定的推广价值。
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| 关 键 词： | 均苯三酚三甲醚 KClO3氧化 硝基还原 醚化 |
| 修稿时间： | 1998-04-29 |
SYNTHESIS OF 1,3,5-TRIMETHOXYBENZENE FROM TNT |
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| HU Yi-min,WANG Xiu-ran. SYNTHESIS OF 1,3,5-TRIMETHOXYBENZENE FROM TNT[J]. Journal of Anhui Normal University(Natural Science Edition), 1999, 22(1): 53-55 |
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| Authors: | HU Yi-min WANG Xiu-ran |
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| Abstract: | Trimethoxybenzene was a new type centre material of medicine. It was supply falls short of demand at home and abroad. The title compound was synthesized by improved methods from TNT.It included 4 steps,Oxidation,reduction,hydrolysis and etherification.This method posesses high yield,simple experimentation,less pollution and widely applied value. |
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| Keywords: | trimethoxybenzene synthesis potash chlorate oxidation nitro reduction etherification |
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