| 一种简易的硫化亚锡微米棒薄膜的合成 |
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| 引用本文： | 杜元宝,韩聪,蔡嫦芳,孟庆哲,孟秀清,吴锋民.一种简易的硫化亚锡微米棒薄膜的合成[J].浙江师范大学学报(自然科学版),2013,36(1):65-67. |
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| 作者姓名： | 杜元宝 韩聪 蔡嫦芳 孟庆哲 孟秀清 吴锋民 |
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| 作者单位： | 浙江师范大学LED芯片研发中心,浙江金华,321004 |
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| 基金项目： | 浙江省自然科学基金资助项目，浙江省新苗人才计划孵化项目 |
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| 摘 要： | 为了得到高纯度的硫化亚锡薄膜,利用恒电压法成功制备了硫化亚锡微米棒薄膜,并将该薄膜在200℃真空退火1 h.结构和形貌分析表明:该薄膜是由2～5μm的细棒组成,并且优先沿着(101)晶面方向生长.拉曼光谱表明该薄膜具有较高的纯度.
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| 关 键 词： | 微米棒 乙二胺四乙酸(EDTA) 恒电压法 温度退火 |
A facile synthesis of SnS microrods films |
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| DU Yuanbao
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HAN Cong
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CAI Changfang
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MENG Qingzhe
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MENG Xiuqing
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WU Fengmin.A facile synthesis of SnS microrods films[J].Journal of Zhejiang Normal University Natural Sciences,2013,36(1):65-67. |
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| Authors: | DU Yuanbao HAN Cong CAI Changfang MENG Qingzhe MENG Xiuqing WU Fengmin |
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| Institution: | (Research Center for Light Emitting Diodes(LED) , Zhejiang Normal University, Jinhua Zhejiang 321004, China) |
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| Abstract: | In order to get SnS with high purity, the SnS microrods films were prepared by constant potential cathodic electro-eposition method and annealed at 200 ℃ under vacuum conditions for 1 h. The structure and morphology analysis showed the films were composed of micro-sized rods. The length of the rods was in a range of 2 - 5 micro and preferentially oriented along the （ 101 ） plane. Raman spectra indicated that the microrods films had a high purity. |
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| Keywords: | microrods EDTA constant potential cathodic method temperature anneal |
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