| 高效液相色谱-库仑电极阵列法检测山茱萸的指纹图谱研究 |
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| 引用本文： | 张延妮,王喆之,杜昱光,李曙光.高效液相色谱-库仑电极阵列法检测山茱萸的指纹图谱研究[J].陕西师范大学学报,2005,33(3):75-77. |
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| 作者姓名： | 张延妮 王喆之 杜昱光 李曙光 |
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| 作者单位： | [1]陕西师范大学生命科学学院,陕西西安710062 [2]中国科学院大连化学物理研究所,辽宁大连116023 |
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| 基金项目： | 国家“十五”科技攻关项目(2001BA701A35) |
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| 摘 要： | 采用高效液相色谱-电化学（库仑电极）阵列检测技术，以马钱素、熊果酸以及齐墩果酸为分析对象，对不同产地山茱萸的指纹图谱进行了初步研究．结果表明，该方法的重现性良好，从不同产地山茱萸指纹图谱比较得出结论，不但佛坪地区样品之间的相似度良好，而且全国各地山茱萸产区的样品也有较好的一致性．该方法简单、准确，可用于对山茱萸的质量控制．
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| 关 键 词： | 山茱萸 高效液相色谱 库仑电极阵列检测技术 指纹图谱 |
| 文章编号： | 1672-4291(2005)03-0075-03 |
| 修稿时间： | 2004年11月30 |
Fingerprint analysis of Macrocarpium officinale by high performance liquid chromatographic coulometric array detection |
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| ZHANG Yan-ni,WANG Zhe-zhi,DU Yu-guang,LI Shu-guang.Fingerprint analysis of Macrocarpium officinale by high performance liquid chromatographic coulometric array detection[J].Journal of Shaanxi Normal University: Nat Sci Ed,2005,33(3):75-77. |
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| Authors: | ZHANG Yan-ni WANG Zhe-zhi DU Yu-guang LI Shu-guang |
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| Institution: | ZHANG Yan-ni~1,WANG Zhe-zhi~1,DU Yu-guang~2,LI Shu-guang~2 |
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| Abstract: | The method of fingerprinu (FP) analysis of Macrocarpium officinale with Loganin,Ursolic acid,Oleanolic acid as the analyues by high performance liquid chromatography (HPLC) coulometric array detection is established. The methodological evaluation shows that the method has a good reproducibility. Comparative studies of HPLC-FPS of Macrocarpium officinale from different sources shows that a close similarity is found not only among acrocarpium officinale from Foping area, but also among Macrocarpium officinale from all over the country. This method is simple and accurate and can be used as a quality control for Macrocarpium officinale. |
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| Keywords: | Macrocarpium officinale high performance liquid chromatography (HPLC) coulometric array detection fingerprint |
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