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间接法合成葡萄糖酸锌及其表征
引用本文:魏巍,王学东,崔玉民.间接法合成葡萄糖酸锌及其表征[J].阜阳师范学院学报(自然科学版),2006,23(4):43-45.
作者姓名:魏巍  王学东  崔玉民
作者单位:1. 阜阳师范学院,化学系,安徽,阜阳,236041;安徽大学,化学化工学院,安徽,合肥,230039
2. 安徽省利辛县第一中学,利辛,236700
3. 阜阳师范学院,化学系,安徽,阜阳,236041
摘    要:介绍了合成葡萄糖酸锌的各种方法,并对其方法的可行性进行了述评.其中间接合成法具有流程短、费用低、产品纯度高的优点.本文在制取葡萄糖酸的基础上,在适宜条件下使其与氧化锌反应制得葡萄糖酸锌.通过红外光谱和熔点测定对产物进行表征,研究了反应条件对产率的影响,得出合成葡萄糖酸锌的最佳条件.

关 键 词:葡萄糖酸锌  葡萄糖酸  红外光谱  熔点
文章编号:1004-4329(2006)04-0014-03
收稿时间:2006-10-25
修稿时间:2006年10月25

Indirect Metatheses Law to Synthesize and Characterize Zinc Gluconate
WEI Wei,WANG Xue-dong,CUI Yu-min.Indirect Metatheses Law to Synthesize and Characterize Zinc Gluconate[J].Journal of Fuyang Teachers College:Natural Science,2006,23(4):43-45.
Authors:WEI Wei  WANG Xue-dong  CUI Yu-min
Institution:1. Department of Chemistry, Fuyang Teachers College, Fuyang 236041,China 2. School of Chemistry and Chemical Engineering of Anhui University, Hefei 230039,China; 3. First Middle School of Lixin City of AnHui Province, Lixin 236700 ,China
Abstract:In this article the methods of synthetic of zinc gluconate have been introduced and the feasibilities of them have been reviewed.We conclude that the better method is the indirect France synthetic zinc gluconate,because this method has the advantage of short flow,low cost and high purity of products.We synthesize the zinc gluconate on the basis of glucose acid and then characterize it through infrared spectral and melting point measurement. A number of conditions have been researched on the effects of zinc gluconate off rate.Finally,we obtained the best condition of synthesizing it.
Keywords:zinc gluconate  glucose acid  infrared spectrum  melting point
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