| CVD金刚石涂层硬质合金工具表面预处理新技术 |
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| 引用本文： | 苗晋琦,宋建华,赵中琴,佟玉梅,唐伟忠,吕反修.CVD金刚石涂层硬质合金工具表面预处理新技术[J].北京科技大学学报,2003,25(5):441-444. |
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| 作者姓名： | 苗晋琦 宋建华 赵中琴 佟玉梅 唐伟忠 吕反修 |
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| 作者单位： | 北京科技大学材料科学与工程学院,北京,100083 |
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| 基金项目： | 国家高技术研究发展计划(863计划);863-715z38-03; |
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| 摘 要： | 研究了利用(KOH K3(Fe(CN)6) H2O和H2SO4 H2O2)两种溶液浸蚀硬质合金基体，分别选择性刻蚀WC和Co的表面预处理过程．在浸蚀过的硬质合金基体上，用强电流直流伸展电弧等离子体CVD法沉积金刚石薄膜涂层．结果表明，两步混合处理法不仅可以有效地去除硬质合金基体表面的钴，而且还显著粗化硬质合金基体表面，提高了金刚石薄膜的质量和涂层的附着力．
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| 关 键 词： | 硬质合金 两步法表面预处理 金刚石薄膜 附着力 等离子体CVD法 |
| 修稿时间： | 2003年1月23日 |
A Pretreatment Method for Adhesion Enhancement of CVD Diamond Coatings on Cemented Carbide Substrates |
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| MIAO Jinqi,SONG Jianhua,ZHAO Zhongqin,TONG Yumei JANG Weizhong,LV Fanxiu Materials Science and Engineering School,University of Science and Technology Beijing,Beijing ,China.A Pretreatment Method for Adhesion Enhancement of CVD Diamond Coatings on Cemented Carbide Substrates[J].Journal of University of Science and Technology Beijing,2003,25(5):441-444. |
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| Authors: | MIAO Jinqi SONG Jianhua ZHAO Zhongqin TONG Yumei JANG Weizhong LV Fanxiu Materials Science and Engineering School University of Science and Technology Beijing Beijing China |
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| Institution: | MIAO Jinqi,SONG Jianhua,ZHAO Zhongqin,TONG Yumei JANG Weizhong,LV Fanxiu Materials Science and Engineering School,University of Science and Technology Beijing,Beijing 100083,China |
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| Abstract: | A method of two-step surface pretreatment utilizing two kinds of solutions to etch respectively the surface WC and Co in cemented carbide substrates was investigated. Diamond films were deposited by means of the High Current Extended DC Arc Plasma CVD Equipment. The results showed that the two-step method can effectively remove the Co in cemented carbide substrates and obviously roughened the surface of the cemented carbide. Enhancements both on the quality and adhesion of the diamond coatings were observed. |
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| Keywords: | two-step surface pretreatment diamond films adhesion cemented carbide |
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