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匀胶法制备TiO_2薄膜的亲水性研究
引用本文:王学敏,王丽君,侯兴刚,李德军,姚琨,沈逸枭.匀胶法制备TiO_2薄膜的亲水性研究[J].天津师范大学学报(自然科学版),2012,32(4):56-60.
作者姓名:王学敏  王丽君  侯兴刚  李德军  姚琨  沈逸枭
作者单位:1. 天津师范大学物理与电子信息学院,天津,300387
2. 扎赉特旗教师进修学校内蒙古兴安盟,137600
基金项目:国家自然科学基金资助项目,天津师范大学博士基金资助项目
摘    要:利用匀胶机制备不同厚度TiO2薄膜,分别用X射线衍射仪(X-ray Diffraction,XRD)、拉曼(Raman)光谱、原子力显微镜(Atomic Force Microscope,AFM)和X射线光电子能谱(X-ray photoelectron Spectroscopy,XPS)表征薄膜微观结构;利用紫外-可见分光光度计(UV-Vis)研究薄膜厚度对光透过率的影响;通过表面接触角测试仪研究TiO2薄膜厚度对其亲水性的影响.实验结果表明:匀胶二层的TiO2薄膜(厚度约为170nm)可达到最佳亲水性;TiO2表面形貌和表面羟基官能团(-OH)的含量会对薄膜亲水性造成影响;继续增加TiO2薄膜厚度不利于改善薄膜亲水性.

关 键 词:TiO2薄膜  亲水性  匀胶法  薄膜厚度  微观结构  透光率

Study on hydrophilicity of TiO2 films prepared by spin coating method
WANG Xue-min , WANG Li-jun , HOU Xing-gang , LI De-jun , YAO Kun , SHEN Yi-xiao.Study on hydrophilicity of TiO2 films prepared by spin coating method[J].Journal of Tianjin Normal University(Natural Science Edition),2012,32(4):56-60.
Authors:WANG Xue-min  WANG Li-jun  HOU Xing-gang  LI De-jun  YAO Kun  SHEN Yi-xiao
Institution:1(1.College of Physics and Electronic Information Science,Tianjin Normal University,Tianjin 300387,China;2.Jalaid Banner Teachers Training School,Hinggan League 137600,Inner Mongolia Autonomous Region,China)
Abstract:TiO2films with different thickness have been deposited on slide glass substrates by spin coating technique.Microstructures of the films are characterized by X-ray diffraction,Raman spectra,atomic force microscopy,X-ray photoelectron spectroscopy,and UV-Vis spectrophotometer is employed to study the effects of the thickness on transmittance.The wettability transformation of the films under UV light irradiation was investigated by using a contact meter.The results demonstrated that the film with two layers(the thickness is about 170nm)has already gotten the best wettability.The hydrophilicity of the films can be influenced by the surface morphology and the content of hydroxyl groups(-OH).Increasing the thickness won’t improve the hydrophilicity of the films when the thickness of the films reaches the threshold value.
Keywords:TiO2film  hydrophilicity  spin coating method  thickness  microstructure  transmittance
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