| Waugh结构(NH4)6[NiMo9O32]·8H2O 的合成及表征 |
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| 引用本文： | 袁华,刘伟,张文育,范小振,谷宁. Waugh结构(NH4)6[NiMo9O32]·8H2O 的合成及表征[J]. 河北师范大学学报(自然科学版), 2006, 30(4): 443-445 |
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| 作者姓名： | 袁华 刘伟 张文育 范小振 谷宁 |
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| 作者单位： | 沧州师范专科学校,化学系,河北,沧州,061001;河北师范大学,化学与材料科学学院,河北,石家庄,050016 |
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| 摘 要： | 以(NH4)6Mo7O24·4H2O,NiSO4·6H2O,(NH4)2S2O8为原料合成了(NH4)6[NiMo9O32]·8H2O(九钼镍杂多酸铵),利用化学分析、差热-热重、红外光谱、紫外光谱等方法对其进行了元素分析及结构的表征.
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| 关 键 词： | Waugh结构 九钼镍杂多酸铵 合成 表征 |
| 文章编号： | 1000-5854(2006)04-0443-03 |
| 收稿时间： | 2005-04-25 |
| 修稿时间： | 2005-06-30 |
Synthesis and Characterization of Ammonium 9-molybdate Nickel Heteropoly Salt with Waugh Structure |
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| YUAN Hua,LIU Wei,ZHANG Wen-yu,FAN Xiao-zhen,GU Ning. Synthesis and Characterization of Ammonium 9-molybdate Nickel Heteropoly Salt with Waugh Structure[J]. Journal of Hebei Normal University, 2006, 30(4): 443-445 |
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| Authors: | YUAN Hua LIU Wei ZHANG Wen-yu FAN Xiao-zhen GU Ning |
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| Abstract: | Ammonium 9-molybdate nickel heteropoly salt with Waugh structure was synthesized by the reaction of nickel sulfate and ammonium heptamolybdate by oxidation of ammonium peroxydisulfate.The(ultimate) analysis and the structure were characterized by IR,UV-Vis,TG-DTA thermal analysis and chemical analysis. |
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| Keywords: | Waugh structure ammonium 9-molybdate nickel heteropoly salt synthesis characterization |
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