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La2O3-CeO2-ZrO2粉的制备及性能
引用本文:刘喜华,毛红,宋波,傅强. La2O3-CeO2-ZrO2粉的制备及性能[J]. 北京科技大学学报, 2004, 26(4): 404-406
作者姓名:刘喜华  毛红  宋波  傅强
作者单位:1. 北京科技大学冶金与生态工程学院,北京,100083
2. 北京科技大学材料科学与工程学院,北京,100083
3. 北京有色金属研究总院,北京,100088
摘    要:利用化学共沉淀法制取锆酸镧(La2Zr2O7,简称LZ)和La2O3-CeO2-ZrO2(简称LCZ)热障涂层喷涂粉,采用电感耦合等离子体光谱仪(ICP-AES)对粉的化学成分进行分析,用X射线衍射仪分析LZ,LCZ的物相组成,用差式扫描量热法研究粉的高温相稳定性.结果表明:LZ,LCZ粉均为烧绿石结构;高温下LZ,LCZ无明显相变.

关 键 词:锆酸镧  热障涂层  化学共沉淀法  性能  Powders  Behavior  相变  烧绿石结构  结果  相稳定性  高温  研究  差式扫描量热法  物相组成  衍射仪  射线  分析  化学成分  光谱仪  等离子体  电感耦合  涂粉  热障涂层
修稿时间:2003-11-20

Preparation and Behavior of La2O3-CeO2-ZrO2 Powders
LIU Xihua,MAO Jinghong,SONG Bo,FU Qiang Metallurgical and Ecological Engineering School,University of Science and Technology Beijing,Beijing ,China Materials Science and Engineering School,University of Science and Technology Beijing,Beijing ,China General Research Institute for Nonferrous Metals,Beijing ,China. Preparation and Behavior of La2O3-CeO2-ZrO2 Powders[J]. Journal of University of Science and Technology Beijing, 2004, 26(4): 404-406
Authors:LIU Xihua  MAO Jinghong  SONG Bo  FU Qiang Metallurgical  Ecological Engineering School  University of Science  Technology Beijing  Beijing   China Materials Science  Engineering School  University of Science  Technology Beijing  Beijing   China General Research Institute for Nonferrous Metals  Beijing   China
Affiliation:LIU Xihua,MAO Jinghong,SONG Bo,FU Qiang Metallurgical and Ecological Engineering School,University of Science and Technology Beijing,Beijing 100083,China Materials Science and Engineering School,University of Science and Technology Beijing,Beijing 100083,China General Research Institute for Nonferrous Metals,Beijing 100088,China
Abstract:Lanthanum zirconate (La2Zr2O7, LZ) and La2O3-CeO2-ZrO2(LCZ) powders for thermal barrier coatings were prepared by coprecipitation. The chemical composition of the powders were analyzed by means of Inductively Coupled Plasma-Atomic Emission Spectrometry (ICP-AES). Crystallogrphic phases were determined by X-ray diffraction technique. Differential Scanning Calorimetry (DSC) was used to analyze the phase stability at high temperatures. The results showed that both LZ and LCZ powders kept the pyrochlore structure and there were no phase transformations for LZ and LCZ at high temperatures.
Keywords:lanthanum zirconate  thermal barrier coatings  coprecipitation
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