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地表水中阴离子表面活性剂测定方法的改进
引用本文:陈力可,刘淼,陈嵩岳,刘南,冷粟,李广柱,杨欣然,王野.地表水中阴离子表面活性剂测定方法的改进[J].东北师大学报(自然科学版),2011,43(2):104-107.
作者姓名:陈力可  刘淼  陈嵩岳  刘南  冷粟  李广柱  杨欣然  王野
作者单位:吉林大学环境与资源学院;扬州大学食品科学与工程学院;
基金项目:科技部专项基金资助项目(2009ZX07208-006-001); 吉林省环保厅资助项目(吉环科字2009)
摘    要:采用0.45μm滤膜代替中速定性滤纸过滤地表水水样.在出现乳化时用干净带圈铜丝代替破乳剂异丙醇破乳,对阴离子型直链烷基苯磺酸钠(LAS)的国标检测方法进行了改进.结果表明:改进后的方法对样品的测定结果与国标方法无明显差异,方法的准确度、精密度均达到质量控制要求;分析步骤更简单,分析效率更高,更加适合测定地表水中的LAs...

关 键 词:地表水  阴离子表面活性剂  方法的改进  破乳  亚甲蓝分光光度法

The improvement on the determination method of anionic surfactant in surface water
CHEN Li-ke,LIU Miao,CHNE Song-yue,LIU Nan,LENG Su,LI Guang-zhu,YANG Xin-ran,WANG Ye.The improvement on the determination method of anionic surfactant in surface water[J].Journal of Northeast Normal University (Natural Science Edition),2011,43(2):104-107.
Authors:CHEN Li-ke  LIU Miao  CHNE Song-yue  LIU Nan  LENG Su  LI Guang-zhu  YANG Xin-ran  WANG Ye
Institution:CHEN Li-ke1,LIU Miao1,CHNE Song-yue1,LIU Nan1,LENG Su1,LI Guang-zhu1,YANG Xin-ran2,WANG Ye1(1.College of Environment and Resources,Jilin University,Changchun 130012,China,2.College of Food Science and Engineering,Yangzhou University,Yangzhou 225001,China)
Abstract:Water samples are filtered through 0.45 m microporous films first.It comprises extracting ion pair with CHCl3 twice,10 mL at a time.When emulsification occurs,It is an effective way to break of the emulsification layer by stirring with a clean copper wire.There is no significant differences between the result of samples determination by using the improved methods and the one by using international standard method.Both of the accuracy and precision of the method meet the quality control requirements,which is...
Keywords:surface water  anionic surfactant  improvement on the method  breaking of emulsification  MBAS spectrophotometry  
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