| 应用2-氨基-4,6-二甲氧基嘧啶合成十一种偶氮化合物 |
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| 引用本文： | 雷厉军,孙西宁,袁晓燕,李志良.应用2-氨基-4,6-二甲氧基嘧啶合成十一种偶氮化合物[J].长沙大学学报,1999,13(4):61-63. |
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| 作者姓名： | 雷厉军 孙西宁 袁晓燕 李志良 |
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| 作者单位： | 1. 湖南大学化学化工学院,长沙,410082
2. 湖南大学化学化工学院,长沙,410082;长沙大学化学系,长沙,410003 |
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| 摘 要： | 以2-氨基-4,6-二甲氧基嘧啶为底物,先对其进行重氮化,再与一些活性芳环偶联,得到十一种偶氮化合物.经以不同有机溶剂重结晶和/或薄层谱分析提纯,测定了溶点及光谱数据.
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| 关 键 词： | 氨基嘧啶 重氮化 偶联反应 偶氮化合物 |
| 文章编号： | 1008-4681(1999)-04-0061-03 |
| 修稿时间： | 1999年7月14日 |
Synthesis and Characterization of Eleven Azo Compounds with 2-Amino-4,6-Dimethyloxy Pyrimidine |
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| Lei Lijun,Sun Xining,Yuan Xiaoyan,Li Zhiliang.Synthesis and Characterization of Eleven Azo Compounds with 2-Amino-4,6-Dimethyloxy Pyrimidine[J].Journal of Changsha University,1999,13(4):61-63. |
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| Authors: | Lei Lijun Sun Xining Yuan Xiaoyan Li Zhiliang |
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| Abstract: | Eleven azo compounds were synthesized using 2-amincr4, 6-dimethyloxy pyrimidine as the mainreactant thriugh the diazotizing and then coupling reaction with hoium nitrite and several aromatic componentscontaining highly active ring. Their structural characterization were then done through infrared spectoscopy andmelting point determination after purification with recrystilization using various organic solvent and/or thin layerchromatography. |
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| Keywords: | Amino pyrimidine Diazotization Coupling Azo compound |
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