离子液体中偶氮化合物的快速合成研究 |
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引用本文: | 陈永魁,姚文惠.离子液体中偶氮化合物的快速合成研究[J].新乡学院学报(自然科学版),2011(3):234-235,239. |
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作者姓名: | 陈永魁 姚文惠 |
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作者单位: | 新乡学院化学与化工学院;新乡学院建筑工程系 |
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摘 要: | 在离子液体中,用NBS(N-溴代丁二酰亚胺)作氧化剂,由不对称N,N’-氢化偶氮苯快速、有效地合成了一系列偶氮化合物。在常温下,用此方法就可快速(1~3 min)合成,且具有绿色、环保的特点。
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关 键 词: | 偶氮化合物 离子液体 NBS |
A Rapid Synthetic Method of Azo Compounds in Ionic Liquid |
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Authors: | CHEN Yong-kuia YAO Wen-hui |
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Institution: | b(a.College of Chemistry and Chemical Engineering;b.Department of Architectural Engineering, Xinxiang University,Xinxiang 453003,China) |
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Abstract: | Using ionic liquid(1-butyl-3-methylimidazolium tetrafluoroborate) and NBS(N-bromosuccinimide) as oxidation system,a series of unsemmetric azo compounds were efficiently prepared from unsymmetric hydrazo compounds.This method has the advantage of being a green process along with a short time. |
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Keywords: | azo compounds ionic liquid NBS |
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