| 饮料中苯甲酸、山梨酸、糖精钠的高效液相色谱快速测定 |
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| 引用本文： | 张家林,李占胜,胡开锋.饮料中苯甲酸、山梨酸、糖精钠的高效液相色谱快速测定[J].齐齐哈尔大学学报(自然科学版),1988(2). |
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| 作者姓名： | 张家林 李占胜 胡开锋 |
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| 作者单位： | 黑龙江省食品卫生监督检验所
(张家林，李占胜)，黑龙江省食品卫生监督检验所(胡开锋) |
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| 摘 要： | 本文报导了一种用高效液相色谱法快速测定饮料中苯甲酸,山梨酸和糖精钠的方法。液相色谱系统包括反相柱(键合C_(18)柱)和紫外检测器(波长254nm;衰减:0.08AUFS);流动相采用甲醇/0.02MNH_4A_0(10/90);流速0.8mL/min;样品经过滤后直接进样,PH可在4—10范围内变化。三种组份的分析约需10分钟。苯甲酸、山梨酸和糖精钠的检测限分别是57ng,2.3ng,和92ng;相对标准偏差分别是1.3—1.8％,1.0％和1.8—3.5％;各种商品饮料的回收率在92—107％内。
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| 关 键 词： | 饮料 高效液相色谱 苯甲酸山梨酸 糖精钠 |
RAPID DETERMINATION OF BENZOIC ACID, SORBIC ACID AND SACCHARIN IN DRINKS BY HPLC |
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| Zhang Jialiu Li Zhausheug Hu Kaifeng.RAPID DETERMINATION OF BENZOIC ACID, SORBIC ACID AND SACCHARIN IN DRINKS BY HPLC[J].Journal of Qiqihar University(Natural Science Edition),1988(2). |
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| Authors: | Zhang Jialiu Li Zhausheug Hu Kaifeng |
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| Institution: | Helongjiang Province Food Hygiene Supervise and Inspect Istijute |
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| Abstract: | A rapid determinatiou method for Benzoic acid, Sorbic acid and Sacchariu in drinks by HPLC is reporled. The LC system includes a reverse-phase columu
(? Bondapak Cl8 column) and an UV detector set at 254 nm and 0.08 AUFS. The mobile phase is methanol/0.02M NH4AC(10/90)at a flow rate of 0.8ml/min. Direct
injection of a filtered liquid sample at PH = 4 -10 allowed detectiou of all the three components in about 10 min. Detection limits for Benzoic acid, Sorbic acid and Saccharin were 57ng, 2.3ng and 92ng respectively. Reletive standard deviations were 1.3-1.8%, 1.0% and 1.8-3.5% respectively. Recoveries ranged from 92 to 107% for varieties of commercial drinks. |
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| Keywords: | beveraye high efficiency Liguid chromatography benzoic acid sorbic acid saccharin sodinrn |
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