| 磷酸铁锰铝分子筛的合成和鉴定 |
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| 引用本文： | 韩淑芸,于桂荣,周铭. 磷酸铁锰铝分子筛的合成和鉴定[J]. 吉林大学学报(理学版), 1990, 0(3) |
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| 作者姓名： | 韩淑芸 于桂荣 周铭 |
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| 作者单位： | 青岛大学化学系，吉林大学化学系，吉林大学化学系 1988年毕业生 |
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| 摘 要： | 用水热法合成了磷酸铁锰铝分子筛(FeMnAPO-5)。通过红外光谱、穆斯堡尔谱等进行了结构和性能研究。实验结果表明,铁和锰已进入了分子筛骨架。
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| 关 键 词： | 分子筛 合成 磷酸铝 铁 锰 |
Synthesis and Identification of FeMnAPO-5 Molecular Sieve |
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| Han Shuyun. Synthesis and Identification of FeMnAPO-5 Molecular Sieve[J]. Journal of Jilin University: Sci Ed, 1990, 0(3) |
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| Authors: | Han Shuyun |
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| Abstract: | The FeMnAPO-5 molecular Sieve was synthesized by hydrothermal method. The structure and properties of FeMnAPO-5 were researched by means of infrared spectra, Mossbauer spectroscopy, high resolution magic-angle-spining solid state ~(31)p and ~(27)Al nuclear magnetic resonance, electron probe, parameters of the unite cell determination, DTA, TG. SEM analysis indicated that its crystal growth were perfect. After adsorption of pyridin the IR spectra showed the presence of both Lewis and Bronsted acid sites. These results illustrate that ferrum and manganese enter into the framework of FeMnAPO-5 molecular sieve. |
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| Keywords: | molecular sieve synthesis aluminophosphate ferrum manganese |
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