| Fe-MCM-41的微波合成及氧化还原行为研究 |
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| 引用本文： | 张东,罗根祥,等.Fe-MCM-41的微波合成及氧化还原行为研究[J].温州大学学报(自然科学版),2001,22(6):19-22. |
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| 作者姓名： | 张东 罗根祥 |
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| 作者单位： | [1]温州师范学院应用化学研究所，浙江温州325003 [2]抚顺石油学院石油化工分院，辽宁抚顺113001 |
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| 基金项目： | 国家自然科学基金资助课题 (编号 2 96740 0 4) |
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| 摘 要： | 以溴代十六烷基吡啶（CPBr)为模板剂，硅溶胶为硅源，利用微波辐射方法合成出了中孔杂原子分子筛Fe-MCM-41。利用XRD、IR、循环伏安法等对Fe-MCM-41的结构进行了表征，结果表明铁元素已进入分子筛骨架，且以Fe^2 形式稳定存在。
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| 关 键 词： | 微波合成 氧化还原行为 Fe-MCM-41 分子筛 溴代十六烷基吡啶 硅溶胶 结征表征 铁 |
Microwave Synthesis and Redox Behaviours Investigation of Fe-MCM-41 |
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| ZHANG Dong,TIAN Yi guang,QIAO Qian.Microwave Synthesis and Redox Behaviours Investigation of Fe-MCM-41[J].Journal of Wenzhou University Natural Science,2001,22(6):19-22. |
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| Authors: | ZHANG Dong TIAN Yi guang QIAO Qian |
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| Abstract: | In this paper,Fe containing mesoporous zeolite Fe MCM 41 was prepared by microwave radiation with cetylpyridinium bromide as templating agent and silica gel as silicon source. The structure of Fe MCM 41 was studied by means of XRD,IR and Cyclic Voltammetry. The results indicated that Fe atoms have been located into the framework of zeolite, and existed stably with F 2 . |
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| Keywords: | Fe MCM 41 Zeolite Synthesis Redox |
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