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DIFFERENTIAL PULSE VOLTAMMETRIC DETERMINATION OF 3,3' 5,5'-TETRAMETHYLBENZIDINE AND ITS ANALOGUES WITH A GLASSY CARBON ELECTRODE
引用本文:丁元晨,仁玉贝.DIFFERENTIAL PULSE VOLTAMMETRIC DETERMINATION OF 3,3' 5,5'-TETRAMETHYLBENZIDINE AND ITS ANALOGUES WITH A GLASSY CARBON ELECTRODE[J].苏州大学学报(医学版),1993,9(2):175-179.
作者姓名:丁元晨  仁玉贝
摘    要:The differential pulse voltarametric ( DPV ) method with a glassy carbon electrode was used for the determination of 3,3‘ 5,5‘-tetramethy lbenzidine ( TMB ) , o-tolidine and benzidine in the acidic media. The pulse amplitude, interval time and scan rate of DPV are optimized to be 50 mV, 0.5 s and 10 mV/s, respectively, The peak current is proportional to the concentration of TMB and its analogues, the linear range is from 10^-8mol/l to 10^-4 mal/l, The electrochemical behaviour of the compounds is discussed, The chemical poisons can be determined directly, or indirectly by the extraction in the waste water of chemical industry and laboratory,

关 键 词:微分脉冲伏安法  测量  3  3'5  5'-四甲基对二氨基联苯  玻碳电极  化学分析
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