DIFFERENTIAL PULSE VOLTAMMETRIC DETERMINATION OF 3,3' 5,5'-TETRAMETHYLBENZIDINE AND ITS ANALOGUES WITH A GLASSY CARBON ELECTRODE |
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引用本文: | 丁元晨,仁玉贝.DIFFERENTIAL PULSE VOLTAMMETRIC DETERMINATION OF 3,3' 5,5'-TETRAMETHYLBENZIDINE AND ITS ANALOGUES WITH A GLASSY CARBON ELECTRODE[J].苏州大学学报(医学版),1993,9(2):175-179. |
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作者姓名: | 丁元晨 仁玉贝 |
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摘 要: | The differential pulse voltarametric ( DPV ) method with a glassy carbon electrode was used for the determination of 3,3‘ 5,5‘-tetramethy lbenzidine ( TMB ) , o-tolidine and benzidine in the acidic media. The pulse amplitude, interval time and scan rate of DPV are optimized to be 50 mV, 0.5 s and 10 mV/s, respectively, The peak current is proportional to the concentration of TMB and its analogues, the linear range is from 10^-8mol/l to 10^-4 mal/l, The electrochemical behaviour of the compounds is discussed, The chemical poisons can be determined directly, or indirectly by the extraction in the waste water of chemical industry and laboratory,
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关 键 词: | 微分脉冲伏安法 测量 3 3'5 5'-四甲基对二氨基联苯 玻碳电极 化学分析 |
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