| 高产率合成5-(4-氨基-苯基)-10,15,20-三苯基卟啉 |
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| 引用本文： | 王金城,赵吉寿,郑启升,侯俭秋,李劲松. 高产率合成5-(4-氨基-苯基)-10,15,20-三苯基卟啉[J]. 云南民族大学学报(自然科学版), 2007, 16(2): 178-181 |
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| 作者姓名： | 王金城 赵吉寿 郑启升 侯俭秋 李劲松 |
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| 作者单位： | 云南民族大学,化学与生物技术学院,云南,昆明,650031 |
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| 摘 要： | 报道了一种非常重要的中间体:5-(4-氨基-苯基)-10,15,20-三苯基卟啉的高产率合成方法,产率达95.2%(以5-(4-硝基-苯基)-10,15,20-三苯基卟啉计),总产率为19.5%(以吡咯计).通过红外光谱、紫外-可见光谱、元素分析对目标产物进行了表征,并且讨论了影响目标产物产率的因素.
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| 关 键 词： | 5-(4-氨基-苯基)-10 20-三苯基卟啉 硝化 还原 合成 |
| 文章编号： | 1672-8513(2007)02-0178-03 |
| 修稿时间： | 2006-10-26 |
The Synthesis of 5 - ( 4-aminophenyl ) -10,15,20-Triphenylporphyrin in High Yield |
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| Wang Jincheng,Zhao Jishou,Zheng Qisheng,Hou Jianqiu,Li Jinsong. The Synthesis of 5 - ( 4-aminophenyl ) -10,15,20-Triphenylporphyrin in High Yield[J]. Journal of Yunnan Nationalities University:Natural Sciences Edition, 2007, 16(2): 178-181 |
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| Authors: | Wang Jincheng Zhao Jishou Zheng Qisheng Hou Jianqiu Li Jinsong |
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| Abstract: | 5-(4-aminopheny1)-10,15,20-tripheny1 porphyrin was synthesized in the yield reached up to 95.2%(calculated by the quantity of 5-(4-aminopheny1)-10,15,20-tripheny1 porphyrin)and the final yield was 19.5%(calculated by the quantity of pyrrole).The products was confirmed by IR,UV-Vis and elemenmtal analysis.And the factors affecting yield of the products were discussed. |
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| Keywords: | 15 |
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