| 微波辐射合成糠酸甲酯的研究 |
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| 引用本文： | 陈钢,周玲妹,徐翠莲,赵士举.微波辐射合成糠酸甲酯的研究[J].河南科学,2007,25(3):386-388. |
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| 作者姓名： | 陈钢 周玲妹 徐翠莲 赵士举 |
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| 作者单位： | 河南农业大学,理学院,郑州,450002 |
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| 摘 要： | 以糠酸和甲醇为原料用微波辐射的方法合成糠酸甲酯.其最佳反应条件为:微波辐射功率320 W,醇酸物质的量比为5∶1,催化剂盐酸用量为糠酸用量的21%,微波辐射时间12 min.结果表明,此法反应时间短,产率达87.4%.
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| 关 键 词： | 微波辐射 糠酸甲酯 合成 |
| 文章编号： | 1004-3918(2007)03-0386-03 |
| 修稿时间： | 2006-09-13 |
Synthesis of Methyl Furoate by Microwave Radiation |
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| CHEN Gang,ZHOU Ling-mei,XU Cui-lian,ZHAO Shi-ju.Synthesis of Methyl Furoate by Microwave Radiation[J].Henan Science,2007,25(3):386-388. |
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| Authors: | CHEN Gang ZHOU Ling-mei XU Cui-lian ZHAO Shi-ju |
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| Institution: | College of Science, Henan Agricultural University, Zhengzhou 450002, China |
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| Abstract: | Methyl furoate is synthesized by furoic acid and methanol under microwave radiation.The optimal conditions are as follows:power of microwave radiation 320 W,molar ratio of alcohol to anhydride 5∶1,amount of catalyst HCl used 21 %,microwave radiation time 12 min.It is found out that,under the optimal conditions,the yield of the product reaches 87.4 %. |
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| Keywords: | microwave radiation methyl furoate synthesis |
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