| 二茂铁乙酮乙酰腙的合成 |
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| 引用本文： | 刘春玲,王丽颖,金静.二茂铁乙酮乙酰腙的合成[J].松辽学刊,2006,27(4):64-65. |
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| 作者姓名： | 刘春玲 王丽颖 金静 |
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| 作者单位： | [1]吉林师范大学化学学院,吉林四平136000 [2]吉林省油田高中,吉林松原138000 [3]松原市油田教育处第11中学,吉林松原138000 |
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| 摘 要： | 以二茂铁与乙酸酐在磷酸催化下反应，合成出乙酰基二茂铁，再用乙酰基二茂铁与乙酰肼作用，得到化合物二茂铁乙酮乙酰腙．通过多步实验确定出腙的最佳合成条件，并通过红外光谱对产物进行鉴定．
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| 关 键 词： | 二茂铁 二茂铁乙酮乙酰腙 合成 |
| 文章编号： | 1000-1840（2006）04-0064-02 |
| 收稿时间： | 2006-09-25 |
| 修稿时间： | 2006年9月25日 |
Synthesis and Characterization of Acetylferrocene Acethydrazone |
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| LIU Chun-ling,WANG Li-ying,JIN Jing.Synthesis and Characterization of Acetylferrocene Acethydrazone[J].Songliao Journal (Natural Science Edition),2006,27(4):64-65. |
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| Authors: | LIU Chun-ling WANG Li-ying JIN Jing |
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| Institution: | 1. College of Chemistry, Jilin Normal University, Siping 136000, China; 2. The High School of Jilin Youtian, Songyuan 138006, China; 3. The 1 lth. Middle School of Oil Field Administrative Office of Scngyuan City, Songyuan 138000, China |
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| Abstract: | Acetylferroeene was synthesized by acetylation of ferrocene with acetic anhydride Further reaction of acetylferrocene with aeethydrazide gave new compound acetylferrocene acethydrazone, the structure of it was authenticated by IR, The reaction conditions were sdudied. |
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| Keywords: | ferroeene aeetylferroeene synthesis |
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