| 改进型过氧钼酸法制备无定形MoO3薄膜 |
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| 引用本文： | 唐怀军,霍海玲,刘文杰,叶立瑗.改进型过氧钼酸法制备无定形MoO3薄膜[J].湖南大学学报(自然科学版),2004,31(5):9-12. |
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| 作者姓名： | 唐怀军 霍海玲 刘文杰 叶立瑗 |
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| 作者单位： | 湖南大学,化学化工学院,湖南,长沙,410082;湖南师范大学,化学化工学院,湖南,长沙,410081 |
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| 基金项目： | 湖南省自然科学基金资助项目(03JJY4005);湖南大学科学基金资助项目 |
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| 摘 要： | 通过金属钼粉与H2O2反应制得过氧钼酸溶胶液后，减压蒸馏除去过氧钼酸溶液中的溶剂水和过量的H2O2，再加入无水乙醇作为溶剂，采用浸泽一提拉法成功地在玻璃表面制备了平整均匀的无定形MoO3薄膜．并通过热分析和X射线衍射分析等对MoO3薄膜的制备机理进行了探讨．
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| 关 键 词： | 三氧化钼 过氧钼酸 薄膜 |
| 文章编号： | 1000-2472(2004)05-0009-04 |
Preparation of Amorphous Molybdenum Oxide Thin Film in Improved Peroxo-polymolybdic Acid Method |
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| TANG Huai-jun,HUO Hai-ling,LIU Wen-jie,YE Li-yuan.Preparation of Amorphous Molybdenum Oxide Thin Film in Improved Peroxo-polymolybdic Acid Method[J].Journal of Hunan University(Naturnal Science),2004,31(5):9-12. |
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| Authors: | TANG Huai-jun HUO Hai-ling LIU Wen-jie YE Li-yuan |
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| Institution: | TANG Huai-jun~1,HUO Hai-ling~1,LIU Wen-jie~2,YE Li-yuan~1 |
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| Abstract: | The solution of peroxo-polymolybdic acid was formed through the reaction of metallic molybdenum with hydrogen peroxide. The solvent water and excess hydrogen peroxide were removed in vacuum distillation process, then the acid was dissolved in absolute alcohol. A smooth amorphous molybdenum oxide thin film was prepared on glass in the dip-coating method. The mechanism of the preparation was investigated through thermal analysis and X-ray diffraction analysis. |
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| Keywords: | molybdenum oxide peroxo-polymolybdic acid thin film |
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