Synthesis and characterization of silica mesoporous material produced by hydrothermal continues pH adjusting path way |
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| Authors: | A. Salemi Golezani A. Sharifi Fateh H. Ahmad Mehrabi |
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| Affiliation: | Department of Metallurgy Engineering, Karaj Branch, Islamic Azad University, Karaj, Alborz, Iran;Department of Metallurgy Engineering, Karaj Branch, Islamic Azad University, Karaj, Alborz, Iran;Department of Metallurgy Engineering, Karaj Branch, Islamic Azad University, Karaj, Alborz, Iran |
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| Abstract: | Mesoporous silica molecular sieves MCM-41 were synthesized under hydrothermal conditions. For this purpose, a solution with a molar coefficient of water, cetyltri-methyl ammonium bromide surfactants as template and sodium silicate as the source of SiO2 are used. Phase formation, morphology and gas absorption properties were investigated by XRD and BET analysis, respectively. The results showed that silica mesoporous material has been successfully synthesized. A favorable special surface and porosity volume together with regular arrangement of nano metric-hexagonal porosities were obtained from this synthesis. Thickness of the wall and average diameter of the pores are 0.8 nm and 4 nm, respectively. |
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| Keywords: | Mesoporous materials MCM-41 Route hydrothermal |
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