| 丙烯酸三溴苯酯的制备 |
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| 引用本文： | 李国防,刘铁良,赵东.丙烯酸三溴苯酯的制备[J].河南科学,2003,21(6):710-712. |
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| 作者姓名： | 李国防 刘铁良 赵东 |
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| 作者单位： | 河南化学研究所,河南郑州,450002 |
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| 摘 要： | 以丙烯酸为原料与亚硫酰氯反应得到丙烯酰氯,丙烯酰氯与2,4,6-三溴苯酚在催化剂存在下反应生成丙烯酸三溴苯酯。利用高压液相色谱测定了产品的纯度,达到99.0%以上。利用红外光谱、质谱等测定了产品的结构,与目标化合物完全相符。
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| 关 键 词： | 丙烯酸三溴苯酯 阻燃剂 丙烯酰氯 三溴苯酚 酯化 |
| 文章编号： | 1004-3918(2003)06-0710-03 |
| 修稿时间： | 2003年6月8日 |
Preparation of tribromophenyl acrylate |
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| Abstract: | The reaction of acrylic acid with thionyl chloride produces acryloyl chloride. Thus, tribromophenyl acrylate is prepared from the reaction of tribromophenol with the as-produced acryloyl chloride in the presence of catalysts. High Pressure Liquid Chromatography analysis gives that the purity of the product is higher than 99.0%. Infrared Spectrum and Mass Spectrum analysis confirms that the structure of the product is just as the same as the expected compound. |
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| Keywords: | tribromophenyl acrylate flame retardant acryloyl chloride tribromophenol esterification |
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