| 含咔唑结构单元新型席夫碱的合成 |
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| 引用本文： | 贾晓丽,王强,宫晓瑞,赵三虎.含咔唑结构单元新型席夫碱的合成[J].江西师范大学学报(自然科学版),2012,0(6):562-564. |
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| 作者姓名： | 贾晓丽 王强 宫晓瑞 赵三虎 |
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| 作者单位： | 忻州师范学院附属外国语中学, 山西 忻州 034000；忻州师范学院化学系, 山西 忻州 034000 |
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| 基金项目： | 山西省高等学校教学改革课题(J2012090);忻州师范学院科研基金(201110)资助项目 |
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| 摘 要： | 以咔唑为起始原料,经Friedel-Crafts烷基化、Ullmann偶联、还原和胺醛缩合系列反应,合成了2个结构新颖的含咔唑结构单元的席夫碱类化合物,所得目标产物及中间体结构经1H NMR、13C NMR和IR 光谱确认.
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| 关 键 词： | 咔唑 1-氯-4-硝基苯 席夫碱 还原 合成 |
The Synthesis of Novel Schiff Base Containing Carbazole Moiety |
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| JIA Xiao-li,WANG Qiang,GONG Xiao-rui,ZHAO San-hu.The Synthesis of Novel Schiff Base Containing Carbazole Moiety[J].Journal of Jiangxi Normal University (Natural Sciences Edition),2012,0(6):562-564. |
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| Authors: | JIA Xiao-li WANG Qiang GONG Xiao-rui ZHAO San-hu |
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| Institution: | 1.Middle School of Foreign Language,Xinzhou Teachers University,Xinzhou Shanxi 034000,China;2.Department of Chemistry,Xinzhou Teachers University,Xinzhou Shanxi 034000,China) |
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| Abstract: | With carbazole as starting material, two novel structure Schiff base containing carbazole moiety were synthesized through a serious of reaction such as Friedel-Crafts alkylation, Ullmann coupling, reduction and con-densation reaction.The structures of object products and intermediates were confirmed by 1H NMR , 13C NMR and IR spectrum. |
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| Keywords: | carbazole 1-chloro-4-nitrobenzene Schiff base reduction synthesis |
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