| N-对硝基苯甲酰四氢噻唑2-硫酮与甘氨酸的反应 |
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| 引用本文： | 李叶芝,崔晓元,黄化民.N-对硝基苯甲酰四氢噻唑2-硫酮与甘氨酸的反应[J].吉林大学学报(理学版),1998(3). |
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| 作者姓名： | 李叶芝 崔晓元 黄化民 |
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| 作者单位： | 吉林大学化学系!长春，130023 |
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| 摘 要： | 在三聚氯氰存在下对硝基苯甲酸与四氢噻唑-2-硫酮反应得到N-对硝基苯甲酰四氢噻唑-2-硫酮．在K2CO3存在下产物与甘氨酸反应得到N-对硝基苯甲酰甘氨酸，与N-甲基甘氨酸反应得到了水解产物对硝基苯甲酸．
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| 关 键 词： | N-对硝基苯甲酰四氢噻唑-2-硫酮 N-对硝基苯甲酰甘氨酸 对硝基苯甲酸 三聚氯氰 |
Reaction of N-p-Nitrobenzoyl-thiazolidine and Glycine |
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| Li Yezhi,Cui Xiaoyuan,Huang Huamin.Reaction of N-p-Nitrobenzoyl-thiazolidine and Glycine[J].Journal of Jilin University: Sci Ed,1998(3). |
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| Authors: | Li Yezhi Cui Xiaoyuan Huang Huamin |
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| Abstract: | p-Nitrobenzoic acid reacted with thiazolidine-2-thione in the presence of cyanuryl chloride as the coupling reagent that the p-nitrobenzoylthiazolidine-2-was obtained. The N-pnitrobenzoylglycine was formed between the reaction of p-nitrobenzoyl-thiazolidine-2 and glycine in the presence of K2CO3, CH3COCH3, H2O. But under the same condition, when N-pnitrobenzoylthiazolidine-2-thione was reacted with N-methyl glycine, the p-nirtobenzoic acid was obtained. |
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| Keywords: | N-p-nitrobenzoylthiazolidine N-p-nitrobenzoylglycine p-nirtobenzoic acid cyanuryl chloride |
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