| TPABr—正丁胺体系中TS—1的合成与表征 |
| |
| 引用本文： | 李钢. TPABr—正丁胺体系中TS—1的合成与表征[J]. 大连理工大学学报, 1998, 38(3): 363-363 |
| |
| 作者姓名： | 李钢 |
| |
| 作者单位： | 大连理工大学碳资源综合利用开放实验室，中国科学院大连化学物理研究所 |
| |
| 基金项目： | 中国石油化工总公司资助,国家自然科学基金,辽宁省博士起动基金,大连市青年基金 |
| |
| 摘 要： | 采用水热晶化法，以ＴＰＡＢｒ为模板剂，正丁胺为碱源合成出钛硅分子筛ＴＳ－１，并探讨了合成过程中的影响因素，利用ＸＲＤ、ＩＲ、ＵＶ－Ｖｉｓ、ＳＥＭ等对合成的分子筛作了表征。
|
| 关 键 词： | 分子筛 TS－1 正丁胺 模板效应 催化剂 |
Synthesis and characterization of TS 1 in presence of TPABr and butylamine |
| |
| Li Gang,Guo Xinwen,Wang Xiangsheng,Li Guangyan. Synthesis and characterization of TS 1 in presence of TPABr and butylamine[J]. Journal of Dalian University of Technology, 1998, 38(3): 363-363 |
| |
| Authors: | Li Gang Guo Xinwen Wang Xiangsheng Li Guangyan |
| |
| Abstract: | The titanium silicalite 1 has been synthesized in the presence of tetrapropylammonium bromide (TPABr) and n butylamine (BuNH 2). Synthesis parameters such as BuNH 2/SiO 2, SiO 2/TiO 2 have been discussed. As synthesized solid has been characterized by XRD, IR, UV Vis and SEM. The template effect in this system has also been investigated by 13 C CP MAS NMR and it is revealed that TPABr is the templating agent and BuNH 2 only acts as a base. |
| |
| Keywords: | molecular sieves/TS 1 TPABr n butylamine template effect |
| 本文献已被 CNKI 维普 等数据库收录！ |
