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丙烯中微量硫化物的定性分析
引用本文:王芳,秦鹏,耿占杰,薛慧峰. 丙烯中微量硫化物的定性分析[J]. 兰州理工大学学报, 2012, 38(1): 55-58
作者姓名:王芳  秦鹏  耿占杰  薛慧峰
作者单位:中国石油兰州化工研究中心,甘肃兰州,730060
摘    要:采用气相色谱-脉冲火焰光度检测器(GC-PFPD)与气相色谱-质谱(G-C-MS)联用技术,分析研究炼油厂精制丙烯原料中的微量硫化物.通过对原料丙烯中的微量硫化物进行富集,采用GC-MS技术与标准品定性,首次从丙烯中检测到异丙基二硫醚和异丙基三硫醚.

关 键 词:气相色谱  脉冲火焰光度检测器  质谱  丙烯  富集  硫化物

Quantitative analysis of trace sulphide in propylene
WANG Fang , QIN Peng , GENG Zhan-jie , XUE Hui-feng. Quantitative analysis of trace sulphide in propylene[J]. Journal of Lanzhou University of Technology, 2012, 38(1): 55-58
Authors:WANG Fang    QIN Peng    GENG Zhan-jie    XUE Hui-feng
Affiliation:(Lanzhou Petrochemical Research Center,PetroChina,Lanzhou 730060,China)
Abstract:A trace sulphide in refined propylene feedstock of refinery were analyzed and investigated by using a combined technology of gas chromatography-pulsed flame photometic detector(GC-PFPD) and gas chromatography-mass spectroscopy(GC-MS).By means of enrichment of the trace sulphide,the isopropyl disulphide ether and isopropyl trisulphide ether in the propylene were first detected by using GC-MS and standard substance.
Keywords:gas chromatograph  pulsed flame photometric detector  mass spectroscopy  propylene  enrichment  sulphide
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