| 酮麝香的合成研究 |
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| 引用本文： | 吕凌,杨莹琴.酮麝香的合成研究[J].信阳师范学院学报(自然科学版),1996,9(3):273-275. |
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| 作者姓名： | 吕凌 杨莹琴 |
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| 作者单位： | [1]华中理工大学汉口分院 [2]信阳师范学院化工系 |
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| 摘 要： | 本文对硝基酮麝香的合成工艺路线进行了改进，对反应条件如催化剂，温度有溶剂的选择进行了优化，其最佳反应条件为：以三氯化铝作催化剂，二氯乙烯作溶剂，并使反应在冰盐溶中进行，从而使产品的产量和质量均有提高。
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| 关 键 词： | 酮麝香 合成 香料 工艺 |
Study on the Synthesis of Musk Ketone |
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| Lu ling Yang, Yingqin et al.Study on the Synthesis of Musk Ketone[J].Journal of Xinyang Teachers College(Natural Science Edition),1996,9(3):273-275. |
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| Authors: | Lu ling Yang Yingqin |
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| Abstract: | This paper reports the technological process of synthesizing 3, 5-dinitro-2, 6-dimethyl-4-tert-butyl acetopherone. The synthetic method was improved. The synthetic conditions such as catalyst, temperature and solvent are selected. The suitable conditions are following: AlCl3 as catalyst, CH2Cl2 as solvent, ice-salt - bath. The yield and quality were improved. |
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| Keywords: | Musk ketone Synthesis |
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