| 二茂铁电解合成法的研究 |
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| 引用本文： | 李助兴 张玉鸿. 二茂铁电解合成法的研究[J]. 内蒙古师范大学学报(自然科学版), 1991, 0(3): 32-35 |
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| 作者姓名： | 李助兴 张玉鸿 |
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| 作者单位： | 内蒙古大学化学系(李助兴)，内蒙古教育学院化学系(张玉鸿) |
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| 摘 要： | 本文研究了以0.5M溴化钠为支持电解质、N,N—二甲基甲酰胺(DMF)为溶剂的体系中电解法合成二茂铁的主要条件。收率按环戊二烯加入量计算为42.6%。测定了产品的熔点、元素百分含量及红外光谱图,所得结果与文献值相符。
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| 关 键 词： | 二茂铁 合成 电解法 |
Studies on Electrolytic Synthesis Method of Ferrocene |
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| Li Zhuxing. Studies on Electrolytic Synthesis Method of Ferrocene[J]. Journal of Inner Mongolia Normal University(Natural Science Edition), 1991, 0(3): 32-35 |
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| Authors: | Li Zhuxing |
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| Abstract: | In the paper primary conditions of electrolytical synthesis of ferrocene were studies in this system, 0.5M NaBr used as supporting electrolyte, N. N-dimethylformamide (DMF) as solvent. The rate of product was 42.6% according to the adding quantity of cyclopentadiene. The m. p of product, percent content of element and IR spectra were determined. These results coincide with those of literature values. |
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| Keywords: | Ferrocene Electrolytic synthesis |
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