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低聚乙二醇的高效液相色谱分析
引用本文:邬安珍.低聚乙二醇的高效液相色谱分析[J].南京师大学报,1992,15(2):54-57,65.
作者姓名:邬安珍
作者单位:南京师大理化中心
摘    要:本文报道了定量分析低聚乙二醇混合物组分的反相高效液相色谱法.此方法以乙腈/水(10/90)作流动相,1cm~3/min 流量(?)浓度洗脱,在195nm 波长光度检测.本方法简便、快速、准确.线性方程y=-(?)031+0.712x,相关系数r=0.9994,回收率97.4%.

关 键 词:高效液相色谱  低聚乙二醇

Assay of mixtures of polyethyl ene glycol oligomers by RP-HPLC
Wu Anzheng.Assay of mixtures of polyethyl ene glycol oligomers by RP-HPLC[J].Journal of Nanjing Normal University(Natural Science Edition),1992,15(2):54-57,65.
Authors:Wu Anzheng
Institution:Chemistry & Physics Centralab
Abstract:This paper reports a simple,rapid and accurate procedure for quantitative determination of mixtures of polyethylene glyeol oilgomers by RP-HPLC.The meth- od employs photomertric detection at 195nm using a reversed phaes C_(18)column with acetonitrile/water(10/90)as the isoeratie cluting system.Linear equation y=-0.081+0.712x,correlation coffieient r=0.9994,the recovery of 97.4%.
Keywords:Reversed phase high performance liquid chromatography(RPHPLC)  Low-wavelength detection  Isocratic clution  Polycthylene glycol oilgomers
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