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1,3-丙二醇的合成及其结构表征
引用本文:彭本军,曾艳.1,3-丙二醇的合成及其结构表征[J].淮北煤炭师范学院学报(自然科学版),2009,30(1).
作者姓名:彭本军  曾艳
作者单位:淮北煤炭师范学院化学与材料科学学院,安徽,淮北,235000
摘    要:文章以无水乙酸钠、3-溴-1-氯丙烷、苄基三乙基氯化铵、无水甲醇、717#离子交换树脂等为原料合成1, 3-丙二醇,并对合成的产物用红外光谱、氢核磁共振波谱进行分析检测.

关 键 词:1  3-丙二醇  3-溴-1-氯丙烷  苄基三乙基氯化铵  相转移催化

The Synthesis and Structural Measurement of 1,3-propanediol
PENG Ben-jun,ZENG Yan.The Synthesis and Structural Measurement of 1,3-propanediol[J].Journal of Huaibei Coal Industry Teachers College(Natural Science edition),2009,30(1).
Authors:PENG Ben-jun  ZENG Yan
Institution:PENG Ben- jun,ZENG Yan (School of Chemistry and Material Science,Huaibei Coal Industry Teachers College,235000,Huaibei,Anhui,China)
Abstract:In this paper,1,3- propanediol is synthesized using anhydrous sodium acetate,3- bromo- 1- chloropropane,anhydrous methanol,benzyl triethyl ammonium chloride and anion exchange resin etc.as materials.In addition,infrared spectra and hydrogen nuclear magnetic resonance are used to determine the chemical structure of production.
Keywords:1  3- propanediol  3- bromo- 1- chloropropane  benzyl triethyl ammonium chloride  phase transfer catalyst  
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