| α,β,γ,δ-四苯基卟啉的合成及其在高效液相色谱中的应用 |
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| 引用本文： | 石志红,傅承光.α,β,γ,δ-四苯基卟啉的合成及其在高效液相色谱中的应用[J].河北大学学报(自然科学版),1997(4). |
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| 作者姓名： | 石志红 傅承光 |
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| 作者单位： | 理化分析中心 |
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| 摘 要： | 合成并提纯了α，β，γ，δ－四苯基卟啉（ＴＰＰ），通过元素分析及一维、二维核磁共振波谱分析确证了化合物的结构。研究了与其有关的理化性质，并将ＴＰＰ用作柱前螯合试剂配以高效液相色谱法实现了Ｃｕ２＋、Ｚｎ２＋、Ｎｉ２＋的同时测定。
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| 关 键 词： | 合成 α.β.γ.δ－四苯基卟啉 显色剂 |
Synthesis of α,β,γ,δ Tetraphenylporphine and its Application in HPLC |
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| Shi Zhihong,Fu Chengguang.Synthesis of α,β,γ,δ Tetraphenylporphine and its Application in HPLC[J].Journal of Hebei University (Natural Science Edition),1997(4). |
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| Authors: | Shi Zhihong Fu Chengguang |
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| Abstract: | α,β,γ,δ Tetraphenylporphine(TPP) was synthesized and purified. The final product was characterized by 1 HNMR, 1 H 1 H Cosy, UV and elemental analysis. As a highly sensitive chromogenic reagent, TPP was used as a precolumn chelating reagent in HPLC determination of trace metal ions. |
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| Keywords: | Synthesis α β γ δ Tetraphenylporphine Chromogenic reagent |
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