| 氯乙酸芳酯的相转移催化合成研究 |
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| 引用本文： | 李英俊,闻利平,孙淑琴,孙亚珍,侯尼波,孙晓晓.氯乙酸芳酯的相转移催化合成研究[J].辽宁师范大学学报(自然科学版),2006,29(4):456-458. |
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| 作者姓名： | 李英俊 闻利平 孙淑琴 孙亚珍 侯尼波 孙晓晓 |
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| 作者单位： | 辽宁师范大学,化学化工学院,辽宁,大连,116029 |
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| 摘 要： | 利用液液相转移催化法合成了10种氯乙酸芳酯．讨论了不同反应条件对产率的影响，通过正交实验。探索出了最佳合成条件．该合成方法具有操作简便，反应温度低、反应时间短．产率较高等优点．
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| 关 键 词： | 氯乙酸芳酯 相转移催化 合成 条件实验 |
| 文章编号： | 1000-1735(2006)04-0456-03 |
| 收稿时间： | 12 28 2005 12:00AM |
| 修稿时间： | 2005年12月28 |
Study on Synthesis of Aryl Chloroacetates with Phase Transfer Catalysis |
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| LI Ying-jun,WEN Li-ping,SUN Shu-qin,SUN Ya-zhen,HOU Ni-bo,SUN Xiao-xiao.Study on Synthesis of Aryl Chloroacetates with Phase Transfer Catalysis[J].Journal of Liaoning Normal University(Natural Science Edition),2006,29(4):456-458. |
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| Authors: | LI Ying-jun WEN Li-ping SUN Shu-qin SUN Ya-zhen HOU Ni-bo SUN Xiao-xiao |
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| Institution: | School of Chemistry and Chemical Engineering, Liaoning Normal University, Dalian 116029, China |
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| Abstract: | Ten aryl chloroacetates were synthesized by liquid-liquid phase transfer catalysis. The most effective syhthetic condition for aryl chloroacetates was obtained experimentlly. The method has advantages of low temperature, short reaction time, simple operation and high yield. |
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| Keywords: | aryl chloroacetate synthesis phase transfer catalysis conditional experiment |
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