| N─苯基─2，2，6，6─四氯环己亚胺的合成 |
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| 引用本文： | 鲁桂林,苗蔚荣,芷术. N─苯基─2，2，6，6─四氯环己亚胺的合成[J]. 齐齐哈尔大学学报(自然科学版), 1994, 0(4) |
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| 作者姓名： | 鲁桂林 苗蔚荣 芷术 |
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| 作者单位： | 齐齐哈尔轻工学院，大连理工大学 |
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| 摘 要： | 本文对医药邻─（２，６─二氯苯胺基）─苯乙酸钠的中间体Ｎ─苯基─２，２，６，６─四氯环己亚胺的合成工艺进行了系统研究，对该反应的催化剂种类、用量、原料配比、缩合温度等。艺条件进行了分析探讨，找出了较佳合成工艺条件，并对产品结构进行了认证。
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| 关 键 词： | N─苯基─2.2.6.6─四氯环己亚胺 |
The Synthesis of N-Phenyl-2, 2, 6, 6- Tetrachlorocyclohexaneimine |
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| Lu Guilin ,Miao Weirong, Zang Shu. The Synthesis of N-Phenyl-2, 2, 6, 6- Tetrachlorocyclohexaneimine[J]. Journal of Qiqihar University(Natural Science Edition), 1994, 0(4) |
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| Authors: | Lu Guilin Miao Weirong Zang Shu |
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| Affiliation: | Lu Guilin ;Miao Weirong; Zang Shu(Qiqihar Light Industry Institute) (Da Lian University) |
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| Abstract: | N-phenly-2, 2, 6. 6-tetrachlorocyclohexaneimine is a intermediate of diclofenac sbdium. The synthetic processes of N-phenly-2, 2. 6. 6-tetrachlorocyclohexaneimine were studied in this paper.the kinds and amount of catalyst used, material ratio,temperature of reaction were discussed. Some outstanding processes were obtained. |
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| Keywords: | N-phenyl-2. 2 6. 6-tetrcho lrocyclohexaneimine |
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