| Cleaner and convenient preparation of 3-（4,6-dimethoxy-pyrimidin-2-yloxy）-2-methyl-phenol |
| |
| 引用本文： | Wen YZ,Fang ZH,Liu WP. Cleaner and convenient preparation of 3-（4,6-dimethoxy-pyrimidin-2-yloxy）-2-methyl-phenol[J]. 浙江大学学报(自然科学英文版), 2004, 5(8): 956-959 |
| |
| 作者姓名： | Wen YZ Fang ZH Liu WP |
| |
| 作者单位： | InstituteofEnvironmentalScience,CollegeofEnvironmental＆ResourceSciences,ZhejiangUniversity,Hangzhou310029,China |
| |
| 摘 要： | Environmental concerns have highlighted the need of cleaner technologies. A cleaner, convenient and selective technology has been developed for the preparation of 3-(4,6-dimethoxy-pyrimidin-2-yloxy)-2-methyl-phenol (DPMP) from 2-methyl-benzene-1,3-diol in water as solvent. The isolated yield of DPMP is up to 86% in good selectivity. The product structure was characterized by conventional methods, 1^H-NMR and MS. This technology belongs to the modern concept of environmentally friendly low wastes or non-wastes technology (LWNWT).
|
| 关 键 词： | 3-（4 6-二甲氧-嘧啶-2-基氧）-2-甲基-苯酚 选择性合成 2-甲基-苯-1 3-二醇 清洁器制备 清洁技术 |
Cleaner and convenient preparation of 3-(4,6-dimethoxy-pyrimidin-2-yloxy)-2-methyl-phenol |
| |
| Wen Yue-Zhong,Fang Zhao-Hua,Liu Wei-Ping. Cleaner and convenient preparation of 3-(4,6-dimethoxy-pyrimidin-2-yloxy)-2-methyl-phenol[J]. Journal of Zhejiang University Science, 2004, 5(8): 956-959 |
| |
| Authors: | Wen Yue-Zhong Fang Zhao-Hua Liu Wei-Ping |
| |
| Affiliation: | Institute of Environmental Science, College of Environmental & Resource Sciences, Zhejiang University, Hangzhou 310029, China. wenyuezhong@zjuem.zju.edu.cn |
| |
| Abstract: | Environmental concerns have highlighted the need of cleaner technologies. A cleaner, convenient and selective technology has been developed for the preparation of 3-(4,6-dimethoxy-pyrimidin-2-yloxy)-2-methyl-phenol (DPMP) from 2-methyl-benzene-1,3-diol in water as solvent. The isolated yield of DPMP is up to 86% in good selectivity. The product structure was characterized by conventional methods, 1H-NMR and MS. This technology belongs to the modern concept of environmentally friendly low wastes or non-wastes technology (LWNWT). |
| |
| Keywords: | |
| 本文献已被 维普 PubMed 等数据库收录！ |
|
