| Cleaner and convenient preparation of 3-（4,6-dimethoxy-pyrimidin-2-yloxy）-2-methyl-phenol |
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| 作者姓名： | Wen YZ Fang ZH Liu WP |
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| 作者单位： | InstituteofEnvironmentalScience,CollegeofEnvironmental＆ResourceSciences,ZhejiangUniversity,Hangzhou310029,China |
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| 摘 要： | Environmental concerns have highlighted the need of cleaner technologies. A cleaner, convenient and selective technology has been developed for the preparation of 3-(4,6-dimethoxy-pyrimidin-2-yloxy)-2-methyl-phenol (DPMP) from 2-methyl-benzene-1,3-diol in water as solvent. The isolated yield of DPMP is up to 86% in good selectivity. The product structure was characterized by conventional methods, 1^H-NMR and MS. This technology belongs to the modern concept of environmentally friendly low wastes or non-wastes technology (LWNWT).
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| 关 键 词： | 3-（4 6-二甲氧-嘧啶-2-基氧）-2-甲基-苯酚 选择性合成 2-甲基-苯-1 3-二醇 清洁器制备 清洁技术 |
Cleaner and convenient preparation of 3-(4,6-dimethoxy-pyrimidin-2-yloxy)-2-methyl-phenol |
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| Wen YZ,Fang ZH,Liu WP.Cleaner and convenient preparation of 3-(4,6-dimethoxy-pyrimidin-2-yloxy)-2-methyl-phenol[J].Journal of Zhejiang University Science,2004,5(8):956-959. |
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| Authors: | Wen Yue-Zhong Fang Zhao-Hua Liu Wei-Ping |
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| Institution: | Institute of Environmental Science, College of Environmental & Resource Sciences, Zhejiang University, Hangzhou 310029, China. wenyuezhong@zjuem.zju.edu.cn |
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| Abstract: | Environmental concerns have highlighted the need of cleaner technologies. A cleaner, convenient and selective technology has been developed for the preparation of 3-(4,6-dimethoxy-pyrimidin-2-yloxy)-2-methyl-phenol (DPMP) from 2-methyl-benzene-1,3-diol in water as solvent. The isolated yield of DPMP is up to 86% in good selectivity. The product structure was characterized by conventional methods, 1H-NMR and MS. This technology belongs to the modern concept of environmentally friendly low wastes or non-wastes technology (LWNWT). |
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