| 胆酸1,2,3-三氮唑衍生物的合成与表征 |
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| 引用本文： | 翟亮亮,陈瑨,霍萃萌,代本才,赵永德.胆酸1,2,3-三氮唑衍生物的合成与表征[J].河南科学,2014(8):1399-1403. |
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| 作者姓名： | 翟亮亮 陈瑨 霍萃萌 代本才 赵永德 |
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| 作者单位： | 1. 河南大学 化学化工学院，河南开封 475001; 河南省科学院 化学研究所有限公司，郑州 450002
2. 河南省科学院 化学研究所有限公司,郑州,450002 |
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| 摘 要： | 以胆酸为起始原料,依次经过酯化反应、3位羟基叠氮化反应、点击反应合成出8个含有4-芳基-1,2,3-三唑环的胆酸衍生物,所有化合物均未见文献报道.所得到的化合物结构均经过IR,1H NMR,13C NMR,ESI-MS,熔点测定等手段的确认.
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| 关 键 词： | -三唑 胆酸 点击反应 |
Synthesis and Characterization of Bile Acid 1,2,3-three Nitrogen Triazole Derivatives |
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| Zhai Liangliang,Chen Jin,Huo Cuimeng,Dai Bencai,Zhao Yongde.Synthesis and Characterization of Bile Acid 1,2,3-three Nitrogen Triazole Derivatives[J].Henan Science,2014(8):1399-1403. |
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| Authors: | Zhai Liangliang Chen Jin Huo Cuimeng Dai Bencai Zhao Yongde |
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| Institution: | Zhai Liangliang, Chen Jin, Huo Cuimeng, Dai Bencai, Zhao Yongde, Zhai Liangliang, Chen Jin, Huo Cuimeng, Dai Bencai, Zhao Yongde ( 1. College of Chemistry and Chemical Enginneering, Henan University, Kaifeng 475001, Henan China： 2. Institute of Chemistry Co. Ltd., Henan Academy of Sciences, Zhengzhou 450002, China) |
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| Abstract: | With bile acid as starting material,eight bile acid derivatives containing 4-aryl-1,2,3-triazole ring were synthesized by esterification,3-OH azide reaction,click reaction. The structures of these compands were characterized by IR,NMR,MS spectra and melting point determination method,and all the compands were confirmed. |
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| Keywords: | 1 2 3-triazole bile acid click reaction |
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