| 1-硝基萘的简单有效合成 |
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| 引用本文： | 李工安,苗江欢,张晓鹏.1-硝基萘的简单有效合成[J].河南师范大学学报(自然科学版),2009,37(5). |
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| 作者姓名： | 李工安 苗江欢 张晓鹏 |
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| 作者单位： | 河南师范大学,化学与环境科学学院,河南,新乡,453007 |
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| 基金项目： | 河南师范大学青年基金，河南师范大学博士科研启动费支持课题 |
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| 摘 要： | 1-硝基萘是合成医药、染料、农药、橡胶防老剂等的重要中间体.报道了一种合成1-硝基萘的简单有效的方法:以单一硝酸(65%~68%)替代传统的由浓硝酸和浓硫酸组成的混酸为硝化剂,在温和条件下方便地制备出1-硝基萘,产率可达86.6%.
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| 关 键 词： | 硝酸 1-硝基萘 萘 硝化 |
Simple and Efficient Synthesis of 1-Nitronaphthalene |
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| LI Gong-an,MIAO Jiang-huan,ZHANG Xiao-peng.Simple and Efficient Synthesis of 1-Nitronaphthalene[J].Journal of Henan Normal University(Natural Science),2009,37(5). |
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| Authors: | LI Gong-an MIAO Jiang-huan ZHANG Xiao-peng |
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| Abstract: | 1-nitronaphthalene is an important intermediate for the synthesis of medicines,dyes,agricultural chemicals and rubber antioxidants.In this paper,a simple and effective method for the synthesis of 1-nitronaphthalene is reported.With sole nitric acid(65%～68%) instead of miscible liquids of concentrated sulfuric acid and nitric acid as nitrating agent,1-nitronaphthalene has been produced expediently in yield of 86.6% under mild conditions. |
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| Keywords: | nitric acid 1-nitronaphthalene naphthalene nitration |
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