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电位溶出分析法测定酱油中铅的含量
引用本文:郭东生,徐玉伦, 姚涛,邓秀芬.电位溶出分析法测定酱油中铅的含量[J].天津理工大学学报,1995(4).
作者姓名:郭东生  徐玉伦  姚涛  邓秀芬
作者单位:天津理工学院化工系
摘    要:将酱油硝化处理后,加入一定量的蒸馏水,用HCl调溶液的PH=2,在恒电位下,使溶液中铅被电解沉积,然后断开电源。用溶液中溶解氧作为氧化剂,使极沉积的铅溶解出来通过溶化出峰进行定量测定。

关 键 词:电位溶出分析法,铅,酱油

POTENTIOMETRIC STRIPPING ANALSIS FOR DETERMINATION OF LEAD CONTENT IN SOY SOUCE
Guo Dongsheng ,Xu Yulun,Yao Tao,Deng Xiufen.POTENTIOMETRIC STRIPPING ANALSIS FOR DETERMINATION OF LEAD CONTENT IN SOY SOUCE[J].Journal of Tianjin University of Technology,1995(4).
Authors:Guo Dongsheng  Xu Yulun  Yao Tao  Deng Xiufen
Institution:Guo Dongsheng ;Xu Yulun;Yao Tao;Deng Xiufen
Abstract:A certain quantity of distilled water is added after the soy souce being nitrafied.The solution of pH=2 is adjusted with HCL and then the lead in the solution will be elec-trodeposited under steady electric potential,then cut off the electricity supply. By usingthe oxygen dissolved in the solution as an oxidizing agent, the electrodeposited lead can besolved in the solution and determined quantitatively with the stripping peaks.
Keywords:potentiometric stripping analysis lead soy souce
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