| 香芹类香料的研制 |
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| 引用本文： | 纪文华,高乾善.香芹类香料的研制[J].山东科学,2011,24(3):83-86. |
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| 作者姓名： | 纪文华 高乾善 |
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| 作者单位： | 山东省分析测试中心，山东 济南 250014 |
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| 摘 要： | 为制备香芹类香料，以香芹酮为原料，采用锌-醇还原、硼氢化钠还原、乙酸酐酯化等方法合成了二氢香芹酮、二氢香芹醇、乙酸二氢香芹酯。重点研究了锌粉在不同溶剂中的还原效果。目标化合物的结构利用核磁共振、质谱做了确证，该合成路线操作简便，收率高（高于80%），成本低，对工业化生产有一定参考价值。
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| 关 键 词： | 香芹酮 香料 合成 |
| 收稿时间： | 2011-01-06 |
Preparation of Celery Spices |
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| JI Wen-hua,GAO Qian-shan.Preparation of Celery Spices[J].Shandong Science,2011,24(3):83-86. |
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| Authors: | JI Wen-hua GAO Qian-shan |
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| Institution: | Shandong Analysis and Test Center, Jinan 250014, China |
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| Abstract: | This paper addressed preparation methods of dihydrocarvone,dihydrocarveol and dihydrocarvyl acetate with carvone as raw material and such steps as reduction,esterification,especially the Zn-ROH reduction.We employed NMR and ESI-MS to determine the structures of these objective compounds.This synthesis process has such positives as low cost and high recovery rate（more than 80%）,and has some references to industrial production. |
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| Keywords: | carvone spice synthesis |
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