| 微波辐射下N-取代乙酰胺的合成 |
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| 引用本文： | 李艳秋,王玉炉,王瑾晔.微波辐射下N-取代乙酰胺的合成[J].河南师范大学学报(自然科学版),2007,35(3):88-90. |
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| 作者姓名： | 李艳秋 王玉炉 王瑾晔 |
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| 作者单位： | 河南师范大学,化学与环境科学学院,河南,新乡,453007;上海有机化学研究所,上海,200032 |
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| 基金项目： | 中国科学院知识创新工程项目 |
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| 摘 要： | 报道了一种简单有效的合成N-取代乙酰胺的新方法.在微波辐射、无溶剂条件下,1.5摩尔比率的乙酸酐和一系列胺发生反应合成15个N-取代乙酰胺,该方法操作简便,反应时间短,产率高.更重要的是该方法适用范围较广(脂肪胺、芳香胺、杂环胺).环境友好.
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| 关 键 词： | 微波 无溶剂 N-取代乙酰胺 合成类型 |
| 文章编号： | 1000-2367（2007）03-0088-03 |
| 修稿时间： | 2006-11-13 |
Solvent-free Synthesis of N-Substituted Acetamides under Microwave Irradiation |
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| LI Yan-qiu,WANG Yu-lu,WANG Jin-ye.Solvent-free Synthesis of N-Substituted Acetamides under Microwave Irradiation[J].Journal of Henan Normal University(Natural Science),2007,35(3):88-90. |
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| Authors: | LI Yan-qiu WANG Yu-lu WANG Jin-ye |
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| Institution: | 1. College of Chemistry and Environmental Science, Henan Normal University, Xinxiang 453007, China 2. Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, Shanghai 200032, China |
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| Abstract: | In this paper,a facile and efficient method was developed for preparing N-substituted acetamides under microwave irradiation.The reaction time is short and the yields are high.What is more,the protocol considerably broadens the scope of amines compared with the microwave-assisted synthesis of amides directly from carboxylic acid. |
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| Keywords: | microwave irradiation solvent-free N-substituted acetamides synthesis |
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