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| H2SO4改性活性炭催化合成橙花素 | |
| 引用本文： | 肖东彩,杨金会,赵艳敏,王伟,刘万毅.H2SO4改性活性炭催化合成橙花素[J].宁夏大学学报(自然科学版),2010,31(2):162-164. |
| 作者姓名： | 肖东彩 杨金会 赵艳敏 王伟 刘万毅 |
| 作者单位： | 1. 宁夏大学能源化工重点实验室,宁夏,银川,750021;银川科技职业学院,宁夏,永宁,750105 2. 宁夏大学能源化工重点实验室,宁夏,银川,750021 3. 银川科技职业学院,宁夏,永宁,750105 4. 宁夏大学能源化工重点实验室,宁夏,银川,750021;宁夏大学化学化工学院,宁夏,银川,750021 |
| 基金项目： | 国家自然科学基金资助项目，国家"973"基金资助项目前期预研专项，教育部科学技术研究重点基金资助项目，宁夏自然科学基金资助项目 |
| 摘 要： | 以活性炭负载硫酸作为一种新型、便宜且有效的环境友好固体催化剂,催化合成了橙花素.考察了反应时间、无水乙醇用量、催化剂用量对合成工艺的影响,确定了最佳反应条件为n（β-萘酚）∶n（无水乙醇）=1∶8,催化剂用量1.2 g,反应时间5 h,反应温度80℃.在此条件下,橙花素产率为91.8%. |
| 关 键 词： | 橙花素 改性活性炭 催化 合成 |
Synthesis of Nerolin Bromelia Catalyzed by Activated Carbon Modified by H2SO4 |
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| Xiao Dongcai,Yang Jinhui,Zhao Yanmin,Wang Wei,Liu Wanyi.Synthesis of Nerolin Bromelia Catalyzed by Activated Carbon Modified by H2SO4[J].Journal of Ningxia University(Natural Science Edition),2010,31(2):162-164. | |
| Authors: | Xiao Dongcai Yang Jinhui Zhao Yanmin Wang Wei Liu Wanyi |
| Institution: | 1.Key Laboratory of Energy Resources and Chemical Engineering,Ningxia University,Yinchuan 750021,China; 2.Yinchuan Vocational College of Science and Technology,Yongning 750105,China; 3.School of Chemistry and Chemical Engineering,Ningxia University,Yinchuan 750021,China) |
| Abstract: | Nerolin bromelia was synthesized in the presence of a new environmentally friendly catalyst H2SO4/carbon.The influences of catalyst＇s dosage,ethanol consumption,and the reaction time on the yield of product have been investigated.Get the optimal reaction conditions as follows： n（β-naphthol）∶n（ethanol）=1∶8,amount of catalyst is 1.2 g,reaction time is 5 h and the temperature is 80 ℃.Under the optimal reaction condition,a 91.8% yield of nerolin bromelia were obtained. |
| Keywords: | nerolin bromelia modified activated carbon catalyst synthesis |
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