| 2,3-环氧蒎烷的合成 |
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| 引用本文： | 俞忠华,周作良,吴卫,陶建华.2,3-环氧蒎烷的合成[J].江西科学,2012,30(4):448-449,472. |
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| 作者姓名： | 俞忠华 周作良 吴卫 陶建华 |
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| 作者单位： | 1. 江西华宇香料化工有限公司,江西抚州,344800
2. 江西省轻工研究所,江西南昌,330029 |
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| 摘 要： | 先以45 wt%的工业H2O2为原料,制备过氧乙酸,然后以过氧乙酸作为环氧化剂,研究反应温度、时间、酸接受体用量、过氧乙酸/α-蒎烯质量比等工艺条件对2,3-环氧蒎烷含量的影响。研究结果表明,在最佳工艺条件下,反应收率可达到89.35%。
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| 关 键 词： | 环氧化 α-蒎烯 2 3-环氧蒎烷 |
The Synthesis of 2,3-Epoxy Pinane |
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| YU Zhong-hua,ZHOU Zuo-liang,WU Wei,TAO Jian-hua.The Synthesis of 2,3-Epoxy Pinane[J].Jiangxi Science,2012,30(4):448-449,472. |
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| Authors: | YU Zhong-hua ZHOU Zuo-liang WU Wei TAO Jian-hua |
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| Institution: | 1.Jiangxi Huayu Aromatic Technology Inc,Jiangxi Fuzhou 344800 PRC; 2.Jiangxi Research Institute of Light Industry,Jiangxi Nanchang 330029 PRC) |
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| Abstract: | Firstly,preparing peracetic acid with 45wt% industrial H2O2 as raw material,and using peracetic acid as epoxidizing agent,to research the influence to 2,3-Pinane Oxide content caused by process conditions,such as reaction temperature,time,acid acceptor dosage,mass ratio of peracetic acid against alpha pinene.The results show that the reaction yield can reach to 89.35% under the optimum process conditions. |
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| Keywords: | Epoxidation Alpha Pinene 2 3-Epoxy Pinane |
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