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高盐雾化器氢化发生新技术及电感耦合等离子体原子发射光谱同时测定沉积物中As、Sb、Se等氢化发生元素
引用本文:王小如,杨原,庄峙厦,黄本立. 高盐雾化器氢化发生新技术及电感耦合等离子体原子发射光谱同时测定沉积物中As、Sb、Se等氢化发生元素[J]. 厦门大学学报(自然科学版), 1994, 0(3)
作者姓名:王小如  杨原  庄峙厦  黄本立
作者单位:化学系分析化学研究所
摘    要:用高盐雾化器(BabingtonNebulizer)作为氢化发生装置与电感耦合等离子体原子发射光谱(ICP/AES)结合同时测定氢化发生元素As、Sb、Se的分析方法,研究了在该氢化发生体系中共存过渡元素对以上元素的氢化发生的干扰及光谱干扰情况,评价了该法的检出限及多次测定的重现性,并用该装置测定了标准沉积物样品中As、Sb、Se的含量.

关 键 词:氢化发生技术,高盐雾化器,沉积物中As、Sb、Se,ICp-AES

Simultaneous Determination of As,Sb,Se in Sediment Samples with Hydride Generation Technique Using High Salt Nebulizer Combined with ICP-AES
Wang Xiaoru,Yang Pengyuan,Zhuang Zhixia,Huang Benli. Simultaneous Determination of As,Sb,Se in Sediment Samples with Hydride Generation Technique Using High Salt Nebulizer Combined with ICP-AES[J]. Journal of Xiamen University(Natural Science), 1994, 0(3)
Authors:Wang Xiaoru  Yang Pengyuan  Zhuang Zhixia  Huang Benli
Abstract:High salt nebulizer(Babington nebulizer)had been applied as a hydridegeneration device. The characteristics of the device was evaluated with the measurements ofAs,Sb,Se detectionm limits and the repeatabities for the mult-measurements. The detectionlimits of As,Sb,Se were 0.2,0.3 and 0.6 hg/ml,respctively. The interferences from thetransition metals on the hytlride generation of those elements were investigated.The systemdeveloped in the present work had been applied to the analysis of standard sediment samples.
Keywords:Hydride generation  High salt nebulizer  As  Sb  Se in sediment sam-ples  ICP-AES  
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