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气相色谱法测定工业甲醇中乙醇的含量
引用本文:李宁辉,刘国军,樊美叶,张春霞,杨扬. 气相色谱法测定工业甲醇中乙醇的含量[J]. 太原科技, 2013, 0(3): 79-80
作者姓名:李宁辉  刘国军  樊美叶  张春霞  杨扬
作者单位:山西焦炭集团益达化工股份有限公司,山西介休032000
摘    要:应用Levenberg—Marqurdt最优化方法,建立了直接测定工业甲醇中微量乙醇的气相色谱分析方法.结果显示,气相色谱法测定甲醇样品中微量乙醇具有准确度高、重现性好和操作简便等优点.本方法的相对标准偏差RSD〈2.06%(n=5),加标回收率为95.20%~100.61%.

关 键 词:气相色谱法  工业甲醇  乙醇

Determination of Content of Ethanol in Industrial by Using Gas Chromatography
Li Ning-hui,Liu Guo-jun,Fan Mei-ye,Zhang Chun-xia,Yang Yang. Determination of Content of Ethanol in Industrial by Using Gas Chromatography[J]. Taiyuan Science and Technology, 2013, 0(3): 79-80
Authors:Li Ning-hui  Liu Guo-jun  Fan Mei-ye  Zhang Chun-xia  Yang Yang
Affiliation:(Yida Chemicals Joint Stock Company, Shanxi Coke Group, Jiexiu 032000 China)
Abstract:The paper was made gas chromatography of direct measurement infinitesimal ethanol in industrial methanol by us-ing optimum theory of Levenberg—Marqurdt. The results indicated that determining infinitesimal ethanol in industrial methanol by using gas chromatography had advantages of high accuracy, good reproducibility and user-friendly control. The relative standard deviation (RSD) of the method was 〈2.06% (n=5), the recovery rate was 95.20% to 100.61%.
Keywords:gas chromatography  industrial methanol  ethanol
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