| 甘草配方颗粒有机氯类农药残留量测定 |
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| 引用本文： | 王爽,曾锐.甘草配方颗粒有机氯类农药残留量测定[J].西南民族学院学报(自然科学版),2013(6):902-906. |
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| 作者姓名： | 王爽 曾锐 |
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| 作者单位： | 西南民族大学民族医药研究院,成都610041 |
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| 基金项目： | 课题得到“十二五”科技支撑计划项目（编号：2012BA127B07）的资助. |
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| 摘 要： | 目的：以气相色谱法对甘草配方颗粒剂中的9种有机氯农药残留量进行检测.方法：样品通过丙酮超声提取,经硫酸净化杂质,用DB-1701P弹性石英毛细管柱分离待测组分,ECD检测器进行检测.结果：9种有机氯农药线性回归方程的相关系数在0.9996～0.9999范围之内,线性关系良好,样品回收率为74.92％～1 15.0％,RSD为0.75％～7.89％.结论：本方法快速、简便、准确,能准确用于甘草配方颗粒中9种有机氯类农药残留的检测.
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| 关 键 词： | 甘草配方颗粒 有机氯农药 气相色谱 |
Determination of organochlorine pesticides residues in radix rhizoma glycyrrhizae formula granule by GC |
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| WANG Shuang,ZENG Rui.Determination of organochlorine pesticides residues in radix rhizoma glycyrrhizae formula granule by GC[J].Journal of Southwest Nationalities College(Natural Science Edition),2013(6):902-906. |
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| Authors: | WANG Shuang ZENG Rui |
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| Institution: | (Ethnic Pharmaceutical Institute, Southwest University for Nationalities, Chengdu 610041, P.R.C.) |
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| Abstract: | Objective： To determine the 9 organochlorine pesticides in radix rhizoma glycyrrhizae formula granule by GC. Methods： To extract the samples with acetone by ultrasonicpurified, and be purified in concentrated sulfuric acid, to separate the analytes by capillary column DB-1701P and determine it by ECD detector. Result： The correlation coefficient to equation of linear regression of 9 organochlorine pesticides is between 0.9096 and 0.9999, the linear relationship is better, the average recovery is 74.92% to115.00%, and the RSD is 0.75% to 7.89%. Conclusion： This method is rapid, simple and accurate, which can determine the 9 organochlorine pesticides residues of Radix Rhizoma Glycyrrhizae tbrmula granule accuracily. |
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| Keywords: | radix rhizoma glycyrrhizae tbrmula granule organochlorine pesticides residues GC |
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